Weather-resistant red ink-jet printing water-based ink and preparation method thereof
An inkjet printing, water-based ink technology, applied in inks, printing, household appliances, etc., can solve problems such as poor weather resistance, and achieve the effect of good fluidity, high weather resistance stability, and clear text and images
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[0031] A kind of preparation method of red ink of the present invention is provided below:
[0032] Step 1: Pour 2% to 4% of the red dye into a beaker, put it on a magnetic stirrer, add 90% to 97% of a solvent composed of distilled water, ethanol, glycerin and ethylene glycol butyl ether, and stir thoroughly for 3 to 5 minutes, then add 0.5% to 3% of surfactant and 0.5% to 3% of polymer, and stir for 10 to 15 minutes;
[0033] Step 2: Stir the above solution until completely dissolved;
[0034] Step 3: Filter the solution completely dissolved in the previous step with filter paper to obtain the product.
[0035] The red ink of the present invention and the commercially available red ink are respectively 12 hours, 24 hours, and 36 hours of ultraviolet light irradiation under a high-pressure mercury lamp, and then select to measure its absorbance under 600nm conditions with a 721 spectrophotometer. The following table shows the change of absorbance of red ink before and after ...
Embodiment 1
[0040] Select respectively:
[0041] NOVACRON reactive red dye 2%;
[0042] 97% solvent, composed of 76% distilled water, 6% ethanol, 12% ethylene glycol butyl ether, and 6% glycerol by weight;
[0043] 0.5% surfactant, composed of cetyltrimethylammonium bromide 5%, sodium laurylsulfonate 40%, OP-10 emulsifier 55% by weight;
[0044] The polymer is 0.5%, and the weight ratio is 25% of polyethylene glycol, 65% of polyvinylpyrrolidone, and 10% of polyvinyl alcohol 400.
[0045] Pour 2% of the red dye into a beaker, put it on a magnetic stirrer, add 97% of a solvent composed of distilled water, ethanol, glycerin and ethylene glycol butyl ether, stir thoroughly for 3 to 5 minutes, then add hexadecane Trimethyl ammonium bromide, sodium dodecyl sulfonate, OP-10 emulsifier to form 0.5% of surfactant and 0.5% of polymer composed of polyvinyl alcohol, polyvinylpyrrolidone and polyethylene glycol 400, stirring 10 to 15 minutes; until the solution is completely dissolved; filter the sol...
Embodiment 2
[0047] Select respectively:
[0048] Champacron Reactive Red Dye 4%;
[0049] 90% solvent, composed of 80% distilled water, 5% ethanol, 10% ethylene glycol butyl ether, and 5% glycerol by weight;
[0050] 3% surfactant, composed of 1% cetyltrimethylammonium bromide, 55% sodium dodecylsulfonate, and 44% OP-10 emulsifier by weight;
[0051] The polymer is 3%, and the weight ratio is 25% of polyethylene glycol 400, 55% of polyvinylpyrrolidone, and 20% of polyvinyl alcohol.
[0052] Pour 4% of the red dye into a beaker, place it on a magnetic stirrer, add 90% of a solvent composed of distilled water, ethanol, glycerin and butyl glycol ether, stir thoroughly for 3 to 5 minutes, then add hexadecane Trimethyl ammonium bromide, sodium dodecyl sulfonate, OP-10 emulsifier composed of 3% of surfactant and 3% of polymer composed of polyvinyl alcohol, polyvinylpyrrolidone, polyethylene glycol 400, stirring 10 to 15 minutes; until the solution is completely dissolved; filter the solution...
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