Extraction method of polysaccharides from morinda officinalis how and application thereof in cigarette
A technology of Morinda officinalis and polysaccharides, which is applied in the extraction method and the application field in cigarettes, can solve the problems that the extraction and purification of Morinda officinalis polysaccharides has not been reported and has not been considered, and can improve the quality of smoking, improve the taste, improve the The effect of smoking quality
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0020] a. Dry the Morinda officinalis officinalis after washing, removing impurities, removing the wood core in the middle of the particles, drying or sun-drying at 60°C, and then crush it to 40 mesh;
[0021] B, get the Morinda officinalis powder obtained in step a, according to water:material (m / m)=20:1, carry out leaching extraction under the condition of 70 ℃, leaching time is 2h;
[0022] c, filter and concentrate the filtrate to 1 / 6 of the volume of the original filtrate;
[0023] d. Add the concentrated solution into absolute ethanol, keep the volume fraction of ethanol at 80%, set aside for 48 hours after mixing, and obtain the crude polysaccharide of Morinda officinalis officinalis after filtering, with a yield of 13.8%
[0024] e, the obtained Morinda officinalis crude polysaccharide of d step is put into water and is redissolved, is mixed with the solution that mass concentration is 5%, then adds the sevag reagent [chloroform: n-butanol (V:V] that volume is 0.8 time...
Embodiment 2
[0029] a. Dry the Morinda officinalis officinalis after washing, removing impurities, removing the wood core in the middle of the particles, drying or sun-drying at 60°C, and then crush it to 40 mesh;
[0030] B, get the Morinda officinalis powder obtained in step a, according to water:material (m / m)=40:1, carry out leaching extraction under the condition of 75 ℃, the leaching time is 1.5h;
[0031] c, filter and concentrate the filtrate to 1 / 10 of the volume of the original filtrate;
[0032] d. Add the concentrated solution to absolute ethanol, keep the volume fraction of ethanol at 80%, set aside to settle for 48 hours after mixing, and obtain the crude polysaccharide of Morinda officinalis after filtering, with a yield of 13.3%
[0033] e, the obtained Morinda officinalis crude polysaccharide of d step is put into water and redissolved, is mixed with the solution that mass concentration is 5%, then adds the sevag reagent [chloroform: n-butanol (V / V) that volume is 0.7 time...
Embodiment 3
[0038] a. Dry the Morinda officinalis officinalis after washing, removing impurities, removing the wood core in the middle of the particles, drying or sun-drying at 60°C, and then crush it to 40 mesh;
[0039] B, get the Morinda officinalis powder obtained in step a, according to water:material=25:1, carry out leaching extraction under 65 ℃ of conditions, leaching time is 1h;
[0040] C, filter, concentrate filtrate to 1 / 8 of former filtrate volume;
[0041] d. Add the concentrated solution to absolute ethanol, keep the volume fraction of ethanol at 80%, set aside for 48 hours after mixing, and obtain the crude polysaccharide of Morinda officinalis after filtering, with a yield of 12.9%;
[0042] e, the obtained Morinda officinalis crude polysaccharide of step d is put into water and is redissolved, is mixed with mass concentration and is 5% solution, then adds the sevag reagent [chloroform: n-butanol (V:V) that volume is 0.7 times of crude polysaccharide solution =4:1], shak...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com