Method for improving wool fire-retardancy with biological enzyme
A bio-enzymatic and flame-retardant technology, which is applied in animal fiber, biochemical fiber treatment, textiles and papermaking, etc., can solve the problem of not being able to endow wool with functions, and achieve the effects of improved flame-retardant performance, increased strength, and less dosage
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Embodiment 1
[0029] Embodiment 1: The wool selected in this example is all-wool veritin, and the selected pretreatment method is KMnO 4 For pretreatment, the selected finishing agent is sodium alendronate.
[0030]Get 2.5g woolen fabric and carry out pretreatment according to following process: woolen fabric is soaked in hot water, potassium permanganate solution oxidation (KMnO 4 3% (owf), penetrant 0.5g / L, temperature 40°C, time 30min, bath ratio 1:20), soaping (45°C, 15min), neutralization cleaning (soda ash 2% (owf)), water rinse , dried at 50°C, decolorized (NaHSO 3 4% (owf), HAc volume fraction 1%, temperature 40°C, time 30min, bath ratio 1:20), washed with water and dried.
[0031] Then the above-mentioned pretreated wool fabric is processed as follows: the fabric is immersed in a buffer solution containing MTG and alendronate (MTG: 20U / g fabric, alendronate: 5% (owf), penetrant 0.5% (owf), temperature 40°C, time 2h, bath ratio 1:20, pH 7.0), washed with water and dried.
[00...
Embodiment 2
[0035] Example 2: The wool selected in this example is all-wool gabardine, the selected pretreatment method is DCCA pretreatment, and the selected finishing agent is sodium pamidronate.
[0036] Take 2.5g of wool fabric and carry out pretreatment according to the following process: cold water immersion, DCCA chlorination treatment (DCCA4% (owf), penetrant 1g / L, pH 3.5, temperature 25 ℃, time 20min, bath ratio 1: 20), 40 Wash with warm water at ℃, dechlorinate (NaHSO 3 6% (owf), pH 4.0, temperature 40°C, time 20min, 1:20), washing with water, adjusting the pH value (Tris-HCl pH 8, temperature 30°C, time 15min, bath ratio 1:25), washing and drying Dry.
[0037] The above-mentioned pretreated wool fabric is processed as follows: the fabric is immersed in a buffer solution containing MTG and sodium pamidronate (MTG: 30U / g fabric, sodium pamidronate: 4% (owf), penetrant 0.5% (owf), temperature 37°C, time 2.5h, bath ratio 1:20, pH 7.5), washed with water and dried.
[0038] The ...
Embodiment 3
[0040] Example 3: The wool selected in this example is Merino Australian wool tops, and the selected pretreatment method is Na 2 SO 3 For pretreatment, the selected finishing agent is phosphoethanolamine.
[0041] Get 2.5g wool tops and carry out pretreatment according to the following process: wool tops are soaked in reducing solution (Na 2 SO 3 3% (owf)), pH8.5, temperature 40°C, time 30min, bath ratio 1:20), washed with water and dried.
[0042] The above-mentioned pretreated tops are processed as follows: the tops are immersed in a buffer solution containing MTG and phosphoethanolamine (MTG: 25U / g fabric, phosphoethanolamine: 3% (owf), penetrant 0.5% (owf), temperature 45°C, time 1.5h, bath ratio 1:20, pH 8), washed with water and dried.
[0043] The samples arranged according to the above process were tested for the following properties, as shown in the following table:
[0044]
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