Immediate throat cool buccal dripping pill and detection method thereof
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A technology for throat diseases and detection methods, applied in respiratory diseases, pill delivery, measuring devices, etc., can solve the problems of toxicity and side effects, toxic side effects, etc.
Inactive Publication Date: 2009-09-02
贵州黄果树立爽药业有限公司
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Before the filing date of this application, the borneol recorded in the "Pharmacopoeia of the People's Republic of China" (1995 edition one) was synthetic borneol, i.e. synthetic borneol, which was mainly processed and synthesized by chemical method
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Embodiment 1
[0046] Embodiment 1 of the present invention: the preparation of Yanli Shuangkou containing dripping pills:
[0047] Take 2.5g of natural borneol (D-borneol), 1.25g of Aina sesame oil, 1.5g of peppermint oil, 0.75g of menthol, 1.5g of monoammonium glycyrrhizinate and 17.5g of polyethylene glycol 6000
[0048] Heat and melt polyethylene glycol 6000, grind natural borneol (D-borneol) and menthol to a viscous liquid, add aina sesame oil, peppermint oil and monoammonium glycyrrhizinate, and mix with melted polyethylene glycol 6000 , stir evenly, transfer to the dripping pill machine and keep warm at 80°C-85°C for 10 minutes; drop into the condensing agent, collect the formed dripping pills, deoil, and obtain the finished dripping pills. This product contains oral administration, 2-4 pills at a time, 4 times a day.
Embodiment 2
[0049] Embodiment 2 of the present invention: the detection method of Yanli Shuangkou containing dripping pills:
[0050] Properties: This preparation is white to light yellow dripping pills; it has a specific aroma, sweet and slightly bitter taste.
[0051] Specific rotation: Take an appropriate amount of this preparation and grind it finely, accurately weigh 5g, put it in a 50ml test tube, add diethyl ether (30ml, 20ml, 10ml) and shake for 3 times, filter, combine the filtrate in an evaporating dish, and store at 50°C Evaporate in a water bath, dissolve the residue in a 25ml measuring bottle with ethanol, and dilute to the mark, and measure according to the law (Appendix VII E of the 2005 edition of the Chinese Pharmacopoeia); the specific rotation is dextrorotatory and not less than +0.2°;
[0052] Identification: (1) The retention time of this preparation in the chromatogram under the item of content determination (1) should be consistent with that of the reference substan...
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Abstract
The invention discloses an immediate through cool buccal dripping pill for treating laryngeal disease and a detection method thereof. The immediate through cool buccal dripping pill is prepared by the following components by weight: 2.5 portions of natural borneol, 1.25 portions of blumea oil, 1.5 portions of dementholised peppermint oil, 0.75 portion of menthol, 1.5 portions of mono-ammonium glycyrrhizinate and 17.5 portions of polyethyleneglycol 6000. Compared with the prior art, the invention adopts the natural borneol to replace moxa pieces or synthesized borneol to prepare the buccal dripping pill for treating laryngeal disease; the obtained dripping pill has obvious curative effect, little toxicity and little side effect; the natural borneol has high content of effective components and is beneficial to producing; and the quality of the immediate through cool buccal dripping pill is improved. In addition, the detection method provided by the invention refers to method of detecting the optical activity of finished product and detecting the content of dextrorotation camphol in the finished product by adopting chiral capillary gas chromatography and has strong specificity, high precision, good stability and accurate measuring result, thereby effectively preventing various adulteration behaviors and effectively ensuring the quality and the curative effect of the buccal dripping pill for treating laryngeal disease.
Description
technical field [0001] The invention relates to a buccal dripping pill for treating throat diseases and a detection method thereof, belonging to the technical field of pharmacy. Background technique [0002] Acute and chronic pharyngitis are common frequently-occurring diseases, Western medicine treatment pharyngitis mainly takes orally and injection anti-inflammatory with various tablets of anti-inflammatory, these treatment methods are relatively poor to the local treatment effect of throat. The Chinese herbal medicine for the treatment of pharyngitis has lozenges and sprays etc., but its curative effect is slow, and dosage is big, and treatment time is long, and effect is not quite satisfactory. The invention patent developed by the applicant is entitled "A Dropping Pill for Treating Throat Diseases and Its Preparation Technology" (trade name; Yanli Shuangkou Han Dropping Pill), and the application number is 97107723.1, which has been authorized. Yanli Shuangkou Handropp...
Claims
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