Tar and harm reducing cellulose balls for cigarette filter tip and preparation thereof
A cigarette filter, coke reduction and harm reduction technology, applied in e-liquid filter elements, tobacco, applications, etc., can solve the problems of long preparation process and weak adsorption capacity
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Embodiment 1
[0023] Cellulose Amination and Cellulose Pelleting
[0024] Add 10g of cellulose and 42g of urea into the reactor for stirring, add 300ml of water and 600ml of xylene, heat at 110°C to separate the water, react for 5 hours, and then raise the temperature. Wash with water, wash with alcohol, separate liquid, remove all organic solvents, and generate cellulose particles. Infrared characterization shows that there are amino groups on the modified cellulose. Take 30-40 mg of the prepared modified cellulose balls and add them to the cigarette filter, analyze the cigarette smoke, and reduce the harmful components of phenols in the cigarette smoke by 19%. Reduce cigarette tar by 2.7mg.
Embodiment 2
[0026] Preparation of cellulose spheres
[0027] Add 10g of cellulose, 42g of urea and 2g of sodium carbonate into the reactor and stir, add 300ml of water and 600ml of cyclohexane, heat at 110°C to separate the water, react for 5 hours, and then raise the temperature. Wash with water, wash with alcohol, separate liquid, remove all organic solvents, and generate cellulose particles. It looks like figure 1 . Add 30-40 mg of the prepared cellulose balls into the cigarette filter, analyze the cigarette smoke, and reduce the cigarette tar by 2.0 mg.
Embodiment 3
[0029] Preparation of cellulose spheres
[0030] Add 10g of cellulose and 2g of calcium carbonate into the reactor and stir, add 300ml of water and 600ml of xylene, heat at 110°C to separate the water, react for 5 hours, then raise the temperature, and remove 90% of the water by dividing the water. Wash with water, wash with alcohol, separate liquid, remove all organic solvents, and generate cellulose particles. Add 30-40 mg of the prepared cellulose balls to the cigarette filter, analyze the cigarette smoke, and reduce the total particle phase of the cigarette by 1.9 mg.
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