Method for extracting insecticidal active material from traditional Chinese medicine feather cockscomb and application thereof
A technology of insecticidal active substances and extraction methods, which is applied in the field of extraction of plant active ingredients, can solve the problems of increasing and less research, and achieve the effects of good control effect, simple process, good social benefits and ecological benefits
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Embodiment 1
[0018] 1. Extraction of the insecticidal active substances of the traditional Chinese medicine Qinglong
[0019] Collect all the plant tissues of Cedarwort, wash them with clean water, put them in an indoor air-drying oven at 45°C, dry them for 24 hours, cool and pulverize them to obtain Cinnamon powder; weigh 2kg of Cinnamon powder and place in In the Soxhlet extractor, the organic solvent methanol was added in a ratio of 1:8 by volume, and the temperature was repeatedly extracted at 65°C for more than 18 hours to obtain the extract of Cymbidium chinense; Concentrate under pressure until the extract becomes a viscous paste, which is the crude extract of green squid; after the crude extract of green squid is dissolved with methanol, press the crude extract of green squid: diatomaceous earth=1:5 weight ratio and silicon The diatomaceous earth is mixed evenly, and the solvent methanol is evaporated to obtain a mixture of the crude extract of Cedarwort - diatomaceous earth; the m...
Embodiment 2
[0029] 1. Extraction of the insecticidal active substances of the traditional Chinese medicine Qinglong
[0030] Collect all the plant tissues of Cedarwort, wash them with clean water, put them in an indoor air-drying oven at 50°C, dry them for 18 hours, cool and pulverize them to get Cinnamon powder; weigh 2kg of Cinnamon powder and place in In the Soxhlet extractor, the organic solvent methanol was added in a ratio of 1:10 by volume, and the temperature was 65°C for more than 18 hours, and the extract was obtained; Concentrate under pressure until the extract becomes viscous paste, which is the crude extract of green squid; after the crude extract of green squid is dissolved in methanol, mix it with silicon The diatomaceous earth is mixed evenly, and the solvent methanol is evaporated to obtain a mixture of the crude extract of Cedarwort - diatomaceous earth; the mixture of the crude extract of Cedarwort - diatomaceous earth is extracted with n-hexane and then extracted with...
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