Organic high molecular composite flocculant and preparation method thereof
A technology of organic polymer and composite flocculant, which is applied in the direction of dehydration/drying/concentrated sludge treatment, etc., can solve the problems of waste of chemicals and complicated treatment process, and achieve the effect of sufficient sources, reasonable preparation and low cost
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Embodiment 1
[0035] Into the 4-ton reactor, the required amount of tap water was added sequentially as a dispersant, and the stirring speed was 65 rpm. Add 16 kg of oxidized starch, add 80 kg of polydimethyldiallyl ammonium chloride (content 40%, intrinsic viscosity 80mL / g), add polyacrylamide (powder solid, ion degree 70% , molecular weight 6 million) 32 kg. The interval between feeding each raw material is 7 minutes, the feeding rate of polyacrylamide is 5Kg / min, and the polyacrylamide is dispersed into the reactor with a high-pressure water gun at the same time. After adding water to the calibrated volume, stir. The total compounding time is 1.5 hours. The compounding temperature in the reactor is 10°C. The polyacrylamide particles are uniformly dispersed and swelled into small micelles of 0.5-2cm until the molecular weight of the liquid reaches 6 million. Reaching 80%, that is, a liquid organic polymer composite flocculant with an effective content of 2% in dry weight of raw materials...
Embodiment 2
[0038] Into the 4-ton reactor, the required amount of tap water was sequentially added as a dispersant, and the stirring speed was 50 rpm. Add 10 kg of phosphate starch, add 54.5 kg of polydimethyldiallyl ammonium chloride (35% content, intrinsic viscosity 100mL / g), and add polyacrylamide A (powder solid, ionic 30%, molecular weight 12 million) 128 kg, add polyacrylamide B (powder solid, ionicity 80%, molecular weight 5 million) 32 kg. The interval between feeding each raw material is 10 minutes, the feeding rate of polyacrylamide is 8Kg / min, and the polyacrylamide is dispersed into the reactor with a high-pressure water gun at the same time. After adding water to the calibrated volume, stir. The total compounding time is 3 hours. The compounding temperature in the reactor is 50°C. The polyacrylamide particles are uniformly dispersed and swelled into small micelles of 0.5-2cm until the molecular weight of the liquid reaches 10 million. Reaching 50%, that is, a liquid organic ...
Embodiment 3
[0041] Into the 4-ton reactor, add the required amount of tap water as a dispersant in sequence, and the stirring speed is 80 rpm. Add 18 kg of cross-linked starch, add 3.6 kg of polydimethyldiallyl ammonium chloride (55% content, intrinsic viscosity 130mL / g), and add polyacrylamide A (powder solid, ionic 40%, molecular weight 10 million) 10 kg, add polyacrylamide B (powder solid, ionicity 60%, molecular weight 8 million) 10 kg. The interval between feeding each raw material is 5 minutes, the feeding rate of polyacrylamide is 3Kg / min, and the polyacrylamide is dispersed into the reactor with a high-pressure water gun at the same time. After adding water to the calibrated volume, stir. The total compounding time is 0.5 hours. The compounding temperature in the reactor is 20°C. The polyacrylamide particles are uniformly dispersed and swelled into small micelles of 0.5-2cm until the molecular weight of the liquid reaches 4 million. Reaching 40%, that is, a liquid organic polymer...
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