Monoclonal antibody resisting human protein RN181, as well as hybridoma cell line 3953 and kit
A technology of hybridoma cell line and monoclonal antibody, which is applied in the direction of anti-enzyme immunoglobulin, biochemical equipment and methods, instruments, etc., and can solve the problem of expression decline
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Embodiment 1
[0026] Embodiment 1: Preparation of anti-RN181 monoclonal antibody
[0027] 1. Inoculate animals
[0028] The hybridoma cells with the preservation number CGMCC3953 in liquid nitrogen were recovered, cultured with 1640 medium containing 10% fetal bovine serum, and the hybridoma cells in the logarithmic growth phase were collected, and the hybridoma cells that had been sensitized with paraffin oil c mice were inoculated intraperitoneally with about 10 hybridoma cells in the logarithmic growth phase 6 indivual. After 10 days, ascitic fluid was collected and centrifuged at 12,000 r / min for 10 min to obtain supernatant, which was filtered with a 0.22 μm filter membrane. Purify the filtered ascites supernatant by Protein-G affinity chromatography: first equilibrate the column with 0.01mol / L PBS for 3 column volumes, dilute the supernatant with 0.01mol / L PBS 1:10, load the sample, 0.01mol / L After washing impurities with PBS, elute with 0.1mol / L glycine hydrochloride buffer (pH2.....
Embodiment 2
[0033] Example 2: Determination of the concentration of anti-RN181 monoclonal antibody
[0034] The anti-RN181 monoclonal antibody prepared by CGMCC3953 hybridoma cells was diluted according to the concentration of 4, 3, 2, 1, 0.5ug / ml, and the paraffin sections of liver cancer tissues and adjacent normal tissues of different pathological grades were tested by immunohistochemistry. The results found that : When the concentration of the monoclonal antibody is 2 μg / ml, the result is specific and clear, and can be well graded for specimens of different pathological grades, see Figure 2-5 .
Embodiment 3
[0035] Example 3: Composition of Immunohistochemical Diagnosis Kit for Primary Liver Cancer (120 pieces in size) and usage method
[0036] 1. The composition of the kit
[0037] 1) 3% H 2 o 2 6ml
[0038] 2) 2 μg / ml monoclonal antibody against human protein RN181 (prepared by CGMCC3953 hybridoma cells) 6ml
[0039] Biotin-labeled goat anti-mouse IgG antibody, streptomycin-labeled horseradish peroxidase (HRP), and DAB chromogenic buffer were purchased from Dako REAL TM Envision TM detection system, in which the volume of each component is 6ml.
[0040] 2. How to use the kit
[0041] The kits are used in the same way as follows:
[0042] 1) 3% H 2 o 2 Drop one drop per piece, incubate at room temperature for 10 minutes;
[0043] 2) Wash with 0.01M PBS (PH7.4) for 5min×3 times;
[0044] 3) Incubate with 2ug / ml monoclonal antibody against human protein RN181 for 1 hour at room temperature;
[0045] 4) Wash with 0.01M PBS (PH7.4) for 5min×3 times;
[0046] 5) One drop ...
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