Foamable styrene system resin particles
A technology of styrene resin and resin particles, applied in the field of foamable styrene resin particles, can solve the problem of incomplete integration of particles and the like
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Embodiment 1
[0081] 40 kg of ion-exchanged water was supplied into an autoclave made of stainless steel and equipped with a stirring device with an inner capacity of 100 liters, and 40 kg of styrene monomer and 40 g of tricalcium phosphate (manufactured by Budenheim Co., Ltd.) were supplied to the ion-exchanged water while stirring the ion-exchanged water. Brand name "C13-09"), 0.5 g of potassium persulfate, 140 g of benzoyl peroxide with a purity of 75% by weight, and 30 g of tert-butyl peroxybenzoate were prepared to prepare a suspension.
[0082] Next, while stirring the above-mentioned suspension at a stirring speed of 200 RPM, the temperature was raised to 90° C. over 1 hour, and the suspension was kept at 90° C. for 6 hours for polymerization, and then 40 g of tricalcium phosphate and 0.4 g of α- Olefin sulfonate (trade name "LIPOLAN PJ-400" manufactured by Lion Corporation), 1600 g of n-pentane and 400 g of isopentane were pressed into it, the temperature of the suspension was raised...
Embodiment 2
[0090] 12-Hydroxystearic acid triglyceride (trade name "K3WAX 500" manufactured by Kawaken Fine Chemicals Co., Ltd.) was replaced with stearic acid triglyceride (trade name "RIKEMAL VT50" manufactured by Riken Vitamin Co., Ltd.) , except that, it was carried out in the same manner as in Example 1.
Embodiment 3
[0092] 0.02 parts by weight of 12-hydroxystearic acid triglyceride (trade name "K3 WAX 500" manufactured by Kawaken Fine Chemicals Co., Ltd.) was replaced with 0.005 parts by weight of 12-hydroxystearic acid triglyceride (Kawaken Fine Chemicals Co. , the trade name "K3WAX 500" manufactured by Ltd.), and 0.02 parts by weight of polyethylene glycol A (trade name "PEG-300" manufactured by NOF Corporation, molecular weight 300) was replaced by 0.01 parts by weight of polyethylene glycol A (NOF Corporation Manufacturing trade name "PEG-300", molecular weight 300), 0.02 parts by weight polyethylene glycol B (trade name "PEG-300" manufactured by NOF Corporation, molecular weight 300) was replaced with 0.03 weight part polyethylene glycol B (Japan It carried out in the same manner as in Example 1, except that the oil company made a brand name "PEG-300", molecular weight 300).
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