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Bone-setting tablet, method thereof for identifying and measuring content

A method of determination, bone bone technology, applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of unfavorable production control and quality supervision of bone bone drugs, unfavorable drug safety for patients, and difficulty in ensuring drug efficacy, etc., to achieve specificity And the effect of good reproducibility, easy control and high accuracy

Active Publication Date: 2012-12-19
JILIN ZHENGHE PHARMA GRP
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AI Technical Summary

Problems solved by technology

The disadvantage is that there are few identification items in the original standard and lack of content determination, which is not conducive to the production control and quality supervision of Jiegu Tablets, and it is difficult to guarantee the efficacy of the drug, which is not conducive to the safety of patients with medication

Method used

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  • Bone-setting tablet, method thereof for identifying and measuring content

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Embodiment Construction

[0020] The identification and content determination methods of bone joint tablets:

[0021] formula:

[0022]

[0023] Preparation method: the above seven flavors, No. 4 copper powder, Aconitum aconitum, frankincense, myrrh, and natural copper are pulverized into fine powder, sieved and mixed,; Chuanxiong, Angelica Zhaoliu extract and the percolation method under the extract ( Chinese Pharmacopoeia 2010 edition one appendix 10) make solvent with 70% ethanol, carry out percolation, ethanol is reclaimed from the percolation liquid, concentrated into paste under reduced pressure. Add the above-mentioned fine powder and auxiliary materials, mix well, make granules, dry below 60°C, press into 1000 tablets, and coat with sugar.

[0024] Identification:

[0025] (1) Take 3 tablets of this product, remove the sugar coating, grind finely, add 5ml of nitric acid, stir well, add 5ml of water, and filter. Take 1ml of the filtrate, add 4ml of water, add 1-2 drops of potassium ferrocy...

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Abstract

The invention relates to a method for preparing and detecting traditional Chinese medicine, in particular to a bone-setting tablet,a method thereof for identifying and measuring contents. The method comprises the following steps of: identifying olibanum, rhizoma ligustici wallichii, angelica and myrrh; and measuring the ferulic acid content. Through sifting of parameter tests, the bone-setting tablet has better chromatographic condition, favorable specificity and repeatability, quickness, economy and practicability; the added method for measuring the ferulic acid content ensures that the method has the advantages of strong specificity and high accuracy, easiness for control as a quality control method of rhizoma ligustici wallichii and angelica, therefore, the product quality of the bone-setting tablet is effectively improved, and the curative effect of the bone-setting tablet product is better ensured.

Description

technical field [0001] The invention relates to a preparation and detection method of a traditional Chinese medicine, that is, a bone joint tablet and a method for its identification and content determination. Background technique [0002] In the prior art, bone joint tablets are included in "Drug Standard Chinese Medicine Prescriptions Second Volume" (WS 3 -B-0402-90), by prescription. It is 2.34g of No. 4 copper powder, 39g of Rhizoma Chuanxiong, 39g of Aconitum aconitum, 39g of Angelica sinensis, 39g of frankincense (roasted with vinegar), 39g of myrrh (roasted with vinegar), and 39g of natural copper (calcined). Preparation method: the above seven flavors, No. 4 copper powder, Aconitum aconitum, frankincense, myrrh, and natural copper are pulverized into fine powder, sieved, and mixed; Chuanxiong, Angelica Zhaoliu extract and the percolation method under the extract ( Chinese Pharmacopoeia 2005 edition one appendix 10) make solvent with 70% ethanol, carry out percolati...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/02G01N30/06G01N21/78G01N30/90
Inventor 姜华
Owner JILIN ZHENGHE PHARMA GRP
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