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Bromothalonil.cuppric nonyl phenolsulfonate compound preparation and application of bromothalonil.cuppric nonyl phenolsulfonate compound preparation to controlling of Ralstonia solanacearum

A technology of bromothalonil and nonylcopper, applied in the field of plant protection, can solve the problems of less fungicides, decreased effect of germ control, and poor effect, and achieve the effects of simple preparation method, significant independent activity, and safe storage and transportation

Inactive Publication Date: 2012-07-18
北京农化生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Generally, it can cause more than 5-50% reduction in production, or even complete production.
At present, there are few fungicides used to prevent and treat tobacco bacterial wilt in the market, and the effect is relatively poor. Although agricultural streptomycin has a good effect, because it is an antibiotic, it is not a medicament advocated by the state, and it has not been used in tobacco at present. Tobacco Bacterial Wilt
In addition, with the prolongation of the drug history, the control effect of a single agent on the bacteria gradually decreased.

Method used

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  • Bromothalonil.cuppric nonyl phenolsulfonate compound preparation and application of bromothalonil.cuppric nonyl phenolsulfonate compound preparation to controlling of Ralstonia solanacearum
  • Bromothalonil.cuppric nonyl phenolsulfonate compound preparation and application of bromothalonil.cuppric nonyl phenolsulfonate compound preparation to controlling of Ralstonia solanacearum

Examples

Experimental program
Comparison scheme
Effect test

preparation example 1

[0065] Preparation Example 1: Preparation of 25.3% bromothalonil·nonyl copper microemulsion

[0066] Take 155 grams of 98% bromothalonil original drug, 110 grams of 92% nonyl copper, add 150 grams of cyclohexanone, 130 grams of ethanol, add 260 grams of HY-6401 emulsifier after completely dissolving, stir evenly, and then stir While adding 195 grams of water, 25.3% bromothalonil·nonylcopper microemulsion was made.

preparation example 2

[0067] Preparation Example 2: Preparation of 30.6% bromothalonil·nonyl copper microemulsion

[0068] Take 110 grams of 98% bromothalonil original drug, 215 grams of 92% nonyl copper, add 190 grams of cyclohexanone, and add 95 grams of sodium dodecylbenzenesulfonate after completely dissolving, nonylphenol polyoxyethylene ether 110 grams, stir evenly, then add 5 grams of ethylene glycol, 5 grams of BHT, and add the above solution to 270 grams of water while stirring to make 30.6% bromothalonil·copper nonyl microemulsion.

preparation example 3

[0069] Preparation Example 3: Preparation of 12.7% bromothalonil·nonyl copper water emulsion

[0070] Get 15 grams of 98% bromothalonil former medicine, 115 grams of 92% nonylcopper, add 150 grams of cyclohexanone, add 55 grams of sodium dodecylbenzenesulfonate after completely dissolving, and sorbitan fatty acid ester 75 grams of polyoxyethylene ether, stir evenly, prepare the oil phase; add 5 grams of ethylene glycol to 585 grams of water, stir evenly, prepare the water phase; under slow stirring, add the oil phase prepared above into the water phase, Made 12.7% bromothalonil · nonyl copper water emulsion.

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Abstract

The invention relates to a bactericidal composition. The bactericidal composition comprises pesticide active ingredients, namely bromothalonil and cuppric nonyl phenolsulfonate, wherein the weight ratio of the bromothalonil to the cuppric nonyl phenolsulfonate is (1:10)-(10:1); and the preferred weigh ratios are (1:8)-(8:1), (1:5)-(5:1), (1:2)-(2:1) and 3:2 (optimal) respectively. The compositioncan be prepared into various formulations such as micro-emulsion, emulsion in water, a suspension and the like; and in the preparation, active ingredients, namely the bromothalonil and the cuppric nonyl phenolsulfonate account for 2 to 70 percent, preferably 5 to 60 percent, more preferably 10 to 50 percent, further preferably 20 to 30 percent and most preferably 25 percent (optimal) of the totalweight of the preparation. Aids used for the processing of the preparation mainly comprise a solvent, a cosolvent, an emulsifier, a dispersant, an antifreezing agent, a stabilizer, a defoaming agent,a thickening agent and the like. The invention also relates to a method for controlling Ralstonia solanacearum by using the composition and application of the composition to the controlling of Ralstonia solanacearum.

Description

technical field [0001] The invention relates to a compound preparation of bromothalonil·nonylcopper, a method and application thereof for preventing and treating tobacco bacterial wilt, and belongs to the technical field of plant protection. Background technique [0002] Brom othalonil (brom othalonil), also known as Huojunqing, the chemical name is 1,2'-dibromo-2,4-dicyanobutane, and its structural formula is: [0003] [0004] Molecular formula C 6 h 6 Br 2 N 2 , molecular weight 265.94, CAS Registry No. 35691-65-7. Bromothalonil is a white solid with a slightly pungent smell, and the industrial product is a yellowish crystal. The melting point is 52.5-54.5°C. Insoluble in water, easily soluble in acetone, alcohol, benzene and other organic solvents. Bromothalonil is a low-toxicity pesticide according to the Chinese Pesticide Toxicity Classification Standard. The acute oral LD50 of male rats is 637mg / kg, and the acute oral LD50 of female rats is 414mg / kg. This v...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N41/08A01N37/34A01P1/00
Inventor 刘勤学
Owner 北京农化生物科技有限公司
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