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Triazine structure contained dye

A disperse dye and monoazo technology, applied in the direction of azo dyes, organic dyes, monoazo dyes, etc., can solve the problems of difficult dyeing depth, poor washing fastness, etc., and achieve excellent moisture resistance, good temperature dependence, sublimation Good fastness effect

Active Publication Date: 2014-02-12
连云港澄鑫化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But they have poor washing fastness and are difficult to dye deep, especially in the case of polyester and spandex blends, it is even more difficult to dye deep, and the washing fastness is even worse

Method used

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  • Triazine structure contained dye

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Add 50 milliliters of sulfuric acid in the flask, add 34.5 grams of o-chloro-p-nitroaniline at room temperature, add 26 grams (100%) of nitrosyl sulfuric acid, and react with diazonium for 4 hours. After the reaction is completed, add 20 milliliters of sulfuric acid, 900 grams of In the mixture of ice water and 62 grams of compounds shown in formula (2),

[0026] Formula (2)

[0027] After the addition, continue to react for 2 hours, add 1000 milliliters of water, slowly rise to 60 ° C and keep warm for 2 hours, cool, and suction filter to obtain the monoazo compound containing triazine structure shown in formula (3):

[0028] Formula (3)

[0029] The polyester fiber is dyed to obtain a red dyed product with excellent fastness properties.

Embodiment 2

[0031] Add 50 ml of sulfuric acid to the three-necked flask, add 52.4 grams of 2,4-dinitro-6-bromoaniline at room temperature, add 26 grams of nitrosyl sulfuric acid (100%), and react with diazonium for 4 hours. After the reaction is completed, add In the mixture of 20 milliliters of sulfuric acid, 900 grams of ice water and 69 grams of compounds shown in formula (4),

[0032] Formula (4)

[0033] After the addition, continue to react for 2 hours, add 1000 milliliters of water, slowly rise to 60 ° C and keep warm for 2 hours, cool, and suction filter to obtain the monoazo compound containing triazine structure shown in formula (5):

[0034] Formula (5)

[0035] The polyester fiber is dyed to obtain a blue dyed product with excellent fastness properties.

Embodiment 3

[0037] Add 50 ml of sulfuric acid into a three-necked flask, add 26 grams of nitrosyl sulfuric acid (100%), add 41.6 grams of 2,4-dinitro-6-cyanoaniline below 10°C, and react with diazonium below 10°C for 4 hours , after the completion of the reaction, add in the mixture composed of 20 milliliters of sulfuric acid, 900 gram of ice water and 74 gram of compound shown in formula (6),

[0038] Formula (6)

[0039] After the addition, continue to react for 2 hours, add 1000 milliliters of water, slowly rise to 80° C. and keep warm for 1 hour, cool, and suction filter to obtain a monoazo compound containing a triazine structure as shown in formula (7):

[0040] Formula (7)

[0041] The polyester fiber is dyed to obtain a blue dyed product with excellent fastness properties.

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PUM

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Abstract

The invention discloses a triazine structure contained monoazo compound and a preparation method and usage thereof. The triazine structure contained monoazo compound is shown as the following formula (1), wherein each perssad is defined in the instruction. Extremely dark dyeing can be obtained when the triazine structure contained dye is used for terylene, terylene superfine fiber, combination fabrics of the terylene superfine fiber and spandex, and the triazine structure contained dye is excellent in each fastness.

Description

A technical field [0001] The invention relates to an azo compound containing a triazine structure, a preparation method and an application thereof, and belongs to the technical field of chemical material preparation. Two background technology [0002] For a long time, the coupling components used as dyes often contain acetanilide groups, such as blue 291:1, purple 93. However, they have poor washing fastness and are difficult to dye deep, especially in the case of polyester and spandex blends, it is even more difficult to dye deep, and the washing fastness is even worse. Therefore, there is a need for an economical new dye with good depth and high wash fastness. Three invention content [0003] The object of the present invention is to provide a monoazo compound containing a triazine structure, which has excellent deep color dyeing performance, light fastness, sublimation fastness and washing fastness, a preparation method and its application. [0004] The technical solu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09B29/36C09B67/38C09B67/22D06P1/18D06P3/54D06P3/85
Inventor 陆建焕谢毅方东
Owner 连云港澄鑫化工有限公司
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