Low refractive index diffuser element having interconnected voids
A low-refractive index layer, diffuser technology, used in diffuser elements, optical elements, instruments, etc., to solve problems such as limited size range and uniformity, and limitations of available material types
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[0061] Comparative example CE-1 is made of polyvinyl alcohol Kuraray PVA-235 and fumed silica dispersion Cab-O-Sperse TM 1020K mixture preparation. PVA was 88% hydrolyzed medium molecular weight polyvinyl alcohol available from Kuraray USA, Houston, TX. Cab-O-Sperse TM 1020K is a non-surface modified basic stable dispersion of L90 fumed silica available from Cabot Corporation, Billerica, MA. In a typical process, 138.8g of 7.2wt% PVA235 aqueous solution was charged into an 800ml plastic beaker (10.0g PVA235 by dry weight), and then 2.0g of 10wt% Tergitol was added TM Min-Foam1X and 1ml concentrated NH 4 OH solution. Tergitol TM Min-Foam 1X is a nonionic surfactant available from Dow Chemical of Midland, MI. Mix the ingredients thoroughly using a stir bar, then add 200g of Cab-O-Sperse TM 1020K, water with 20 wt% fumed silica and an additional 162g deionized (DI) water. The components were thoroughly mixed under low shear using an air mixer to reduce foaming. After mix...
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