Iron-oxide-ore-containing heavy oil hydrogenation catalyst, and preparation and application thereof

A heavy oil hydrogenation and catalyst technology, which is applied in the direction of organic compound/hydride/coordination complex catalyst, physical/chemical process catalyst, petroleum industry, etc., can solve the problems of poor stability and dispersion performance, and achieve good mixing ability and dispersion Good performance and good heavy oil hydrogenation catalytic activity

Active Publication Date: 2013-09-11
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The purpose of the present invention is to provide a heavy oil hydrogenation catalyst containing iron oxide ore powder,

Method used

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  • Iron-oxide-ore-containing heavy oil hydrogenation catalyst, and preparation and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0024] Example 1

[0025] Weigh 40 g of diesel oil, add 0.9 g of organic bentonite (Jiangsu Huate New Material Company, the mass fraction of organic matter is 15-20%), and homogenize on a shearing machine. Then heat and stir on an oil bath at 60° C. for 2 hours, add 0.5 g of analytically pure ethylene glycol, stir until homogeneous, and then cool to room temperature to obtain dispersion medium A.

Example Embodiment

[0026] Example 2

[0027] Weigh 38 g of kerosene, add 0.8 g of fumed silica (with a particle size of less than 1 μm), and homogenize with a shearing machine. Then, it was heated and stirred on an oil bath at 50° C. for 2 hours, 0.2 g of glycerol was added, stirred to a homogeneous phase, and then cooled to room temperature to obtain dispersion medium B.

Example Embodiment

[0028] Example 3

[0029] Take the limonite ore powder whose average particle size is less than 20 μm, weigh 6.0 g and place it in a test tube. Weigh 12.0 g of Dispersing Medium A in the same test tube, stir and shake the glass rod, and let it stand for 6 hours after the powder is evenly infiltrated without significant sedimentation. A catalyst C1 was obtained.

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Abstract

The invention relates to an iron-oxide-ore-containing heavy oil hydrogenation catalyst, and preparation and application thereof. The heavy oil hydrogenation catalyst is composed of iron oxide ore powder and a dispersion medium, wherein the iron oxide ore powder accounts for 5-70 wt% of the catalyst; and on the basis of the dispersion medium, the dispersion medium contains 80-99 wt% of base oil, 0.05-10 wt% of solid thickening rheological agent and 0.05-10 wt% of polar additive. The heavy oil hydrogenation catalyst provided by the invention has the advantages of high catalytic-activity solid content, favorable mixing capacity with heavy oil raw oil, and favorable catalytic effect in heavy oil hydrocracking or modification in a suspension bed or slurry-state bed.

Description

technical field [0001] The invention relates to a heavy oil hydrogenation catalyst. More specifically, it is a catalyst for heavy oil hydrogenation containing iron oxide ore powder, as well as the preparation method and application of the catalyst. Background technique [0002] With the gradual scarcity of conventional oil resources, the proportion of heavy oil, especially low-quality heavy oil, in the total oil is increasing. How to efficiently convert heavy oil has become a huge challenge in the energy field. The heavy oil referred to above includes asphalt, oil sands, shale oil, residual oil with a boiling point higher than 524°C, etc. Its characteristics are: high asphaltene and residual carbon content, high metal nickel and vanadium content, the total content is generally not less than 200μg / g, high S and N compound content, and high apparent viscosity at normal temperature and pressure. Inferior heavy oil is prone to clogging pipelines and reactors and producing coke...

Claims

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Application Information

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IPC IPC(8): B01J31/28C10G47/04
Inventor 郜亮宗保宁温朗友俞芳慕旭宏董明会
Owner CHINA PETROLEUM & CHEM CORP
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