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74results about How to "Good dispersion performance" patented technology

Method for preparing spherical superfine silver powder by using chemical reduction method

The invention provides a method for preparing spherical superfine silver powder by using a chemical reduction method, using ascorbic acid to reduce silver nitrate and using gelatin as a dispersing agent. An ascorbic acid solution and a silver nitrate solution with certain concentrations are respectively prepared with the mole ratio of the amounts of the silver nitrate to the ascorbic acid of 2:1; the silver nitrate is dropwise added in the ascorbic acid solution while stirring, the gelatin is dropwise added when sediments start to generate, and the pH value of a reaction solution is regulated by ammonia water; the reaction solution is filtered and washed after titration, the sediments are taken out, dried in a drying oven and then is put in a muffle furnace to be heated to 350 DEC C, and then impurities are removed through heat preservation and thermal treatment. The prepared silver powder is in a spherical shape or a shape similar to a ball and has the advantages of smooth surface, less agglomeration and favorable dispersion; the impurity content is less than 5*10-4, the specific surface area is from 0.8 to 1.5 m2.g-1, the thermal gravitation is less than 2%, the tap density is about 4g.cm-3, and the particle size distribution is from 0.5 to 3 mum. The method can be used for producing electrode slurry for sheet-type elements, silver paste for the glass of saloon cars, and the like, and has important industrial application value.
Owner:KUNMING UNIV OF SCI & TECH

Starch-based graft copolymer coal water slurry dispersant and preparation method thereof

The invention provides a starch-based graft copolymer coal water slurry dispersant and a preparation method thereof. The method comprises steps that: a 10% to 20% starch aqueous suspension is heated; an oxidizing agent which takes 0.1% to 5% of the mass of starch is added to the aqueous suspension of starch for carrying out an oxidization reaction for 10 to 60min; the mixture is heated to a temperature of 80 to 95 DEG C, and the mixture is gelatinized for 20 to 60min while maintaining the temperature; the temperature of the mixture is reduced to 40 to 70 DEG C, and meanwhile mixed monomer and an initiator are dropped into the mixture; the mixture is heated to a temperature of 80 to 95 DEG C, and is subject to a reaction while maintaining the temperature for 20 to 120min; the temperature is reduced to 20 to 40 DEG C, and the pH value of the mixture is regulated to 7-9 by using a sodium hydroxide solution. The dispersant is a viscous emulsion with a color of light yellow to off-white, a solid content of 25 to 35%, a pH value of 7 to 9, and a viscosity of 30 to 150mPa.s. According to the invention, strong dispersibility of styrene and carboxylic salt is fully utilized. Hydrogen bonding effect of polyhydroxy on starch straight chains upon hydrones is adopted, such that the storage stability of the coal water slurry is improved, the dispersibility of the coal water slurry is good, and the stationary phase of the coal water slurry is long-lasting.
Owner:SHAANXI UNIV OF SCI & TECH

Viscosity reduction type polycarboxylate concrete admixture and preparation method thereof

The invention discloses a viscosity reduction type polycarboxylate concrete admixture and a preparation method thereof. The polycarboxylate concrete admixture contains the following synthetic raw materials: low molecular weight segmented modified unsaturated polyoxyethylene ether comonomer A, an unsaturated carboxylic acid comonomer B, alkylphenol ethoxylate C, an initiator, a reducing agent, a chain transfer agent, caustic soda liquid and water, wherein the mass ratio of the synthetic raw materials is as follows: a ratio of the low molecular weight segmented modified unsaturated polyoxyethylene ether comonomer A to the unsaturated carboxylic acid comonomer B to the alkylphenol ethoxylate C to the initiator to the reducing agent to the chain transfer agent to the caustic soda liquid to the water is (320-420):(24-36):(3-10):(1-5):(0.5-3):(0.5-4):(20-50):(400-500). The viscosity reduction type polycarboxylate concrete admixture disclosed by the invention has the characteristics of excellent dispersion property, obvious viscosity reduction effect, and excellent cement adaptability, and the product is simple in process, safe, reliable and stable in performance, does not contain any chloride ion, does not have any Corrosion damage on reinforcement and is environment-friendly.
Owner:广东瑞安科技实业有限公司

Polyacrylate adhesive containing traditional Chinese medicine oil microcapsule as well as preparation method and application

The invention provides a polyacrylate adhesive containing a traditional Chinese medicine oil microcapsule, and aims to solve the problem that an adhesive needs to be additionally added into an existing traditional Chinese medicine oil microcapsule in a sorting process of textiles. The polyacrylate adhesive containing the traditional Chinese medicine oil microcapsule is a compound of the traditional Chinese medicine oil microcapsule and the polyacrylate emulsion. The preparation method of the polyacrylate adhesive containing the traditional Chinese medicine oil microcapsule comprises the steps that the traditional Chinese medicine oil microcapsule of which the wall material contains (methyl) acrylic acid is prepared by utilizing a complex coacervation method; and the polyacrylate adhesive containing the traditional Chinese medicine oil microcapsule is prepared by using an in-situ emulsion polymerization method. The polyacrylate adhesive containing the traditional Chinese medicine oil microcapsule can be applied in the textiles, and be directly used after being diluted according to the technological requirements and the adhesive is not additionally added; the sorted textiles have a good antibacterial effect and are in wash durability.
Owner:临泉县嘉鸿装饰工程有限公司

Method for producing high-intensity fine denier fiber from scrap material and returned material of polyester bottles

The invention relates to a method for producing high-intensity fine denier fiber from a scrap material and a returned material of polyester bottles. The method is characterized by comprising the following steps of: after the material is dried for the second time and the water content of the material is controlled below 80 ppm, adding the following chemical additives in percentage by mass: 0.02 to 0.04 percent of OB-1 brightening agent, 0.02 to 0.04 percent of barium stearate and 0.04 to 0.06 percent of titanium white into the material, uniformly stirring the mixture, and fusing and stirring the mixture in a screw rod at a high temperature and extruding the mixture; arranging a mixing region at the tail end of a screw extruder, wherein the length of the mixing region H is 3 to 4 times the sleeve diameter D of the screw extruder; and raising the temperature of a heating region of a screw rod sleeve from conventionally 260-310 DEG C to 285-340 DEG C. A product produced by the method belongs to high-intensity fine denier fiber; the linear density of the fiber is less than or equal to 1.55 dtex and the breaking strength of the fiber is CN/dtex is more than or equal to 5.8; and the quality of the product reaches or is close to the quality standard of similar chopped fiber produced by melt direct spinning. The method has the advantages of reliving the situation of material shortage for users, saving the consumption of national resource consumptions, fulfilling the aim of mutual benefits and bringing considerable economic benefit to enterprises.
Owner:广东秋盛资源股份有限公司

Preparation method of modified superfine graphene

The invention discloses a preparation method of modified superfine graphene. The preparation method includes the following steps that (1), graphene is subjected to grinding, specifically, the grapheme is placed in a grinder and is ground to obtain graphene pasty material; (2), the graphene pasty material is subjected to stage treatment, specifically, the graphene pasty material is put into a high-speed centrifugal settling type grader, the graphene pasty material whose particle diameter is less than or equal to 1 [mu]m is concentrated in the middle of the grader, and is stored in a storage tank after being led out; and (3), the graphene pasty material whose particle diameter is less than or equal to 1 [mu]m is subjected to kneading treatment, specifically, the graphene pasty material whose particle diameter is less than or equal to 1 [mu]m is put into a kneading reaction device, a surface treating agent is added, the kneading treatment is conducted, the superfine graphene is obtained after being kneaded, and in the period, the accumulating density of superfine graphene powder is controlled within 0.5-1.2. According to the preparation method, the prepared modified superfine graphene particles have the characteristics of being good in dispersing performance, low in accumulating density and the like. Partial shielding and disturbing to electromagnetic waves and wireless signals are achieved, and the effect of gaining advantages in information competition is realized.
Owner:江苏华力索菲新材料有限公司

Low-surface tension hyperbranched shrinkage reduction type polycarboxylate superplasticizer and preparation method thereof

The invention relates to the technical field of building additives and in particular to a low-surface tension hyperbranched shrinkage reduction type polycarboxylate superplasticizer and a preparationmethod thereof. The preparation method comprises the following steps: putting an unsaturated polyether, a polyhydroxy polymer and a hyperbranched shrinkage reduction functional monomer and water intoa container, mixing at 20-60 DEG C, adding an initiator solution, a chain transfer agent solution and an unsaturated acid solution, keeping the temperature for a certain time, and adjusting the pH value of the obtained reaction product to 6.0-7.0 by using an alkali substance, thereby obtaining the low-surface tension hyperbranched shrinkage reduction type polycarboxylate superplasticizer. As a great amount of the shrinkage reduction functional monomer is introduced into a polycarboxylic acid molecular structure through copolymerization, the polycarboxylic acid molecular structure has a shrinkage reduction function chain segment, a steric hindrance segment and an adsorption group segment, the prepared superplasticizer product has low surface tension, unification of shrinkage reduction and dispersing performance of concrete can be achieved with a low doping amount, the concrete can be prevented from shrinkage cracking, then the durability of the concrete can be improved, and practical application values are great.
Owner:KZJ NEW MATERIALS GROUP CO LTD +1
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