Isotropic graphite material and manufacturing method
A graphite material and iso-directional technology, applied in the field of directional graphite materials and their manufacturing, can solve the problems of cracking, cracks on the surface of the graphite material, long process processing time, etc., achieve good iso-directionality, shorten the process time, Good effect of crack defects
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Embodiment 1 to Embodiment 4
[0046] Embodiment 1 to embodiment 4 use mesocarbon microsphere B as raw material, wherein the basic information of mesocarbon microsphere B is listed in Table 1 (its TI is 99.4%, QI is 98.9%, average particle diameter (D 50 ) is 21 μm; Sinosteel Carbon Chemical Co., Ltd.).
[0047] About 55 grams of the above-mentioned mesocarbon microspheres B without pretreatment are filled in a cylindrical rubber mold (mold wall thickness 1.0 mm) with an inner diameter of about 25 mm, wherein the filling height of the mesocarbon microspheres in the mold is It is about 140mm. After compacting with a homogeneous rubber cover on the mold cover, carry out simple packaging (for example, use electrical tape to wrap it tightly) to avoid contamination caused by pressurized liquid intruding into the mold inadvertently during the cold equalization operation.
[0048] The above-mentioned mold containing mesophase carbon microspheres is placed in a cold isostatic pressure equipment (CL4.5-22-30, Nikki...
Embodiment 5
[0052] Embodiment 5 uses mesocarbon microsphere G as raw material, wherein the basic information of mesocarbon microsphere G is listed in Table 1 (its TI is 99.0%, QI is 98.6%, average particle diameter (D 50 ) is 24 μm; China Steel Carbon Chemical Co., Ltd.).
[0053] Under the protection of nitrogen gas, the mesophase carbon microspheres G were placed in the temperature range of 200° C. to 500° C. for 6 hours of heat treatment. Thereafter, it was pulverized using an air-induced pulverization equipment (ALG-2, Lingguang Industrial Co., Taiwan). After that, the particle size analyzer (Multisizer TM 3, Beckman Coulter, Inc., U.S.A.) analyzed the pulverized powder material of mesocarbon microspheres, the average particle size (D 50 ) is about 7 μm.
[0054] Next, about 860 grams of the above-mentioned pretreated powder were filled in a cylindrical rubber mold with an inner diameter of 100 mm (mold wall thickness 4.0 mm), and the filling height of the pulverized powder in the ...
Embodiment 6
[0060] Embodiment 6 uses mesophase carbon microspheres M as raw material, wherein the basic information of mesocarbon microspheres M is listed in Table 1 (its TI is 96.9%, QI is 95.0%, average particle diameter (D 50 ) is 24 μm; China Steel Carbon Chemical Co., Ltd.).
[0061] Mesocarbon microspheres M were pulverized using an air-induced pulverizing device (the same as that used in Example 5) before use; the particle size analyzer (same as that used in Example 5) was used to analyze the mesocarbon microspheres through Average particle size after pulverization (D 50 ) is about 5 μm.
[0062] Next, about 250 grams of the above-mentioned pretreated powder was filled in a cylindrical rubber mold with an inner diameter of 71 mm (mold wall thickness 1.0 mm), and the filling height of the pulverized powder in the mold was about 118 mm.
[0063] The above-mentioned mold filled with mesophase carbon microspheres pretreated by crushing is placed in a cold equal pressure equipment (CL...
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