A kind of super low temperature resistant fully synthetic diesel engine oil and its preparation method
A fully synthetic, diesel engine technology, used in the petroleum industry, lubricating compositions, base materials, etc., to achieve excellent ultra-low temperature unbounded startability
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[0032] The present invention also provides a preparation method of ultra-low temperature resistant fully synthetic diesel engine oil, comprising the following steps:
[0033] 1) Under the catalytic polymerization of toluene, alkylbenzene and polymer binary ethylene propylene hydrocarbon are stirred and reacted at 80-110°C for 2-4 hours to obtain base oil;
[0034] 2) Stir molybdenum anti-wear energy-saving agent and dispersant at 40-60°C for 1-2 hours, then add boronized ashless dispersant, anti-oxidant and anti-corrosion agent and detergent and stir at 40-60°C for 1-2 hours 2 hours, get compound additive;
[0035] 3) Stir the base oil obtained in step 1 and the composite additive obtained in step 2 at 30-50°C for 1-2 hours, and perform coarse and fine filtration to obtain super low-temperature resistant fully synthetic diesel engine oil.
[0036] Among them, the polymer binary ethylene propylene hydrocarbon is a binary ethylene propylene rubber obtained by copolymerization o...
Embodiment 1
[0039] The invention provides a super low temperature resistant fully synthetic diesel engine oil, which consists of the following components in parts by weight:
[0040] 80 parts of alkylbenzene, 2 parts of polymer binary ethylene propylene hydrocarbon, 2 parts of toluene, 3 parts of high alkali value synthetic calcium sulfonate, 2.5 parts of monoalkenyl succinimide, 1.5 parts of thiadiazole derivatives, boron 3.5 parts of chemical ashless dispersant, 1.8 parts of molybdenum dialkyldithiophosphate.
[0041] Diesel engine oil preparation method:
[0042] 1) Mix the high-molecular binary ethylene propylene hydrocarbon with alkylbenzene in an enamel reaction kettle, drop toluene into it with a dropper, and react under toluene catalytic polymerization at 95°C for 3 hours, then vacuum extract the toluene to obtain the base oil; the index detection results of base oil are as shown in table 1;
[0043] 2) Stir dialkylmolybdenum dithiophosphate and monoalkenyl succinimide at 50°C f...
Embodiment 2
[0050] The invention provides a super low temperature resistant fully synthetic diesel engine oil, which consists of the following components in parts by weight:
[0051] 75 parts of alkylbenzene, 1 part of polymer binary ethylene propylene hydrocarbon, 1 part of xylene, 2 parts of calcium alkyl salicylate, 2 parts of polyisobutylene bis-succinimide, 1 part of zinc salt of sulfur phosphorus secondary alcohol , 3 parts of boride ashless dispersant, 0.5 parts of sulfur phosphorus nitrogen molybdenum complex.
[0052] Diesel engine oil preparation method:
[0053] 1) Mix the high-molecular binary ethylene propylene hydrocarbon with alkylbenzene in an enamel reaction kettle, drop xylene into it with a dropper, under the catalytic polymerization of toluene, stir and react at 110°C for 2 hours, and then vacuum extract the toluene to obtain Base oil; each index detection result of base oil is as shown in table 1;
[0054] 2) Stir the sulfur phosphorus nitrogen molybdenum complex wi...
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