A kind of manganese zinc soft magnetic ferrite material and preparation method thereof
A manganese-zinc soft magnet and oxygen body technology is applied in the field of manganese-zinc soft magnetic ferrite materials, which can solve the problems of inability to achieve high saturation magnetic flux density and increased material loss, and achieve high saturation magnetic induction intensity, convenient operation, and low The effect of loss
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Embodiment 1
[0026] 1. Weigh according to the formula
[0027] Main component: 53.5mol% Fe 2 o 3 , 8.8mol% of ZnO, 37.7mol% of MnO;
[0028] Additive: 0.035wt%CaCO 3 , 0.005wt% SiO 2 , 0.025wt%V 2 o 5 , 0.025wt%Nb 2 o 5 , 0.01wt%ZrO 2 , the mass percent of each component in the additive formula is calculated relative to the total mass of the main component.
[0029] 2. Put the weighed main components into the mixer in turn for 45 minutes, mix them in the flip vibrating ball mill for 25 minutes, pre-fire in the rotary sintering furnace at 1050°C for 50 minutes, and then pass through the straight row Vibrating ball mill for primary crushing for 25 minutes, feeding flow rate of 10-15Kg / min, and then secondary crushing in vertical sand mill for 100 minutes, adding additives at the same time of secondary crushing, after secondary crushing, the slurry The particle size is 1.2-1.5 μm. After the mixture is sprayed and granulated, it is pressed into a ring-shaped sample with an outer dia...
Embodiment 2
[0033] 1. Weigh according to the formula
[0034] Main component: 52.7mol% Fe 2 o 3 , 5.5mol% of ZnO, 41.8mol% of MnO;
[0035] Additive: 0.05wt%CaCO 3 , 0.01wt%SiO 2 , 0.05wt%V 2 o 5 , 0.03wt%Nb 2 o 5 , 0.03wt%ZrO 2 , 0.3wt%NiO, 0.1wt%Co 3 o 4 The mass percent of each component in the additive formula is calculated relative to the total mass of the main component.
[0036] 2. Put the weighed main components into the mixer in turn for 45 minutes, mix them in the flip vibrating ball mill for 25 minutes, pre-fire in the rotary sintering furnace at 1050°C for 50 minutes, and then pass through the straight row Vibrating ball mill for primary crushing for 25 minutes, feeding flow rate of 10-15Kg / min, and then secondary crushing in vertical sand mill for 100 minutes, adding additives at the same time of secondary crushing, after secondary crushing, the slurry The particle size is 1.2-1.5 μm. After the mixture is sprayed and granulated, it is pressed into a ring-shaped s...
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