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A method for controlling furnace bottom rise in titanium carbide slag production process

A technology of production process and furnace bottom rising, applied in the field of metallurgy, can solve problems such as furnace bottom rising, and achieve the effect of solving furnace bottom rising, reducing furnace opening time, and improving output and production efficiency

Active Publication Date: 2016-02-03
PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The purpose of the present invention is to provide a control method suitable for solving the problem of furnace bottom rise when titanium-containing raw materials are prepared by high-temperature carbothermal reduction reaction in electric furnace or submerged arc furnace.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0045] A dust-collecting material in the production process of titanium metallurgy is used as the titanium-containing raw material, in which TiO 2 The content is 27.29%, and the rest are oxides of iron, calcium, magnesium, silicon, and aluminum. The titanium-containing raw material and carbonaceous reducing agent are evenly mixed and then added to a submerged arc furnace with a rated power of 3200KVA. The height of the bottom slope of the submerged arc furnace is 75mm and the rated current is 21735A. In the melting and heating stage, the control current is 16000-18000A, and the input power at this time is controlled at 2100-2600KVA; at the carbonization reduction stage, the control current is 13000-16000A, and the input power at this time is controlled at 1700-2000KVA; stage, the control current is 17000-19000A, the input power at this time is controlled at 2400-3000KVA and the control duration is 20-30min.

[0046] Continuously smelting 33 heats through the above control met...

example 2

[0048] The titanium-containing blast furnace slag is used as the titanium-containing raw material, and coke is used as the carbonaceous reducing agent. The titanium-containing raw material and the carbonaceous reducing agent are added to an electric furnace with a rated power of 5000kVA. The furnace bottom slope height of the electric furnace is 135mm, and the rated current is . 12230A. In the melting and heating stage, the control current is 9000-11000A, and the input power at this time is controlled at 2500-4000KVA; at the carbonization reduction stage, the control current is 7000-9000A, and the input power at this time is controlled at 2250-3250KVA; In the first stage, the control current is 10000-11000A to carry out the final temperature rise reaction on the slag, the input power at this time is controlled to be 3750-4750KVA, and the furnace is opened rapidly at the same time, and the opening time of the slag outlet is controlled to be 5-12min.

[0049] Continuously smelti...

example 3

[0051] High-titanium blast furnace slag is used as the titanium-containing raw material, and coke is used as the carbonaceous reducing agent. The titanium-containing raw material and the carbonaceous reducing agent are added to an electric furnace with a rated power of 8500KVA and a rated current of 25000A.

[0052] The initial weight of the electric furnace is 130 tons. Before the above-mentioned technology of controlling the rise of the furnace bottom was mastered at the beginning, the bottom of the electric furnace continued to rise, and the weight of the electric furnace reached 142.6 tons, that is, the bottom residue was about 10 tons.

[0053] The slag removal operation is carried out first. The normal charging amount of the electric furnace is 18 tons, and the maximum charging amount is 25 tons. After the bottom of the furnace rises, the charging amount is controlled to be 6-12 tons, and the amount of reducing agent is reduced to the normal charging amount. 1 / 2~2 / 3 of th...

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PUM

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Abstract

The invention discloses a method for controlling the rising of a furnace bottom in a production process of a titanium carbide slag. When the rising furnace bottom is not higher than the upper limit position of a slag outlet of a reaction furnace, a first input power is adopted in power transmission in the fusion temperature rise period, wherein the first input power is 50-90% of the rated power of the reaction furnace; the input power is reduced to a second input power for power transmission in the carbonization reduction period, wherein the second input power is 45-65% of the rated power of the reaction furnace; the input power is increased to a third input power for power transmission in the slag discharge period, wherein the third input power is 75-95% of the rated power of the reaction furnace, and the amount of residuals in the furnace bottom is controlled not to be higher than the upper limit position of the slag outlet of the reaction furnace after the slag discharge. When the rising furnace bottom is higher than the upper limit position of the slag outlet of the reaction furnace, the slugging operation is implemented, and the production is carried out after the amount of the residuals in the furnace bottom is not higher than the upper limit position of the slag outlet of the reaction. The method provided by the invention effectively solves the problem of rising of the furnace bottom caused by deposition of titanium carbide in the reduction process.

Description

technical field [0001] The invention belongs to the technical field of metallurgy, and relates to a process for preparing titanium carbide-containing materials by using a carbothermal reduction method, and more specifically, relates to a method for controlling furnace bottom rise in the production process of titanium carbide slag. Background technique [0002] Titanium carbide is used to make cermets, cutting tool materials, wear-resistant refractory materials, heat-resistant alloys, hard alloys, etc. due to its excellent properties such as high temperature resistance, wear resistance, corrosion resistance, high strength, high hardness, and thermal conductivity. It is widely used in high-tech industries such as metallurgical mines, machinery, chemicals, microelectronics, aerospace and national defense. [0003] Titanium carbide can be prepared by high-temperature carbothermal reduction reaction in electric furnace or submerged arc furnace by using raw materials containing ti...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B31/30C01B32/921
Inventor 赵青娥张继东杨仰军周玉昌黄家旭李良
Owner PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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