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Method for detecting potassium dichromate by utilizing graphene quantum dot probe

A technology of graphene quantum dots and potassium dichromate, applied in the field of chemical detection, can solve problems such as unseen, and achieve the effects of low detection limit, good biocompatibility and high fluorescence intensity

Inactive Publication Date: 2014-09-10
GUANGXI TEACHERS EDUCATION UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

But so far, there are still no reports on the use of graphene quantum dot fluorescent probes for potassium dichromate detection.

Method used

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  • Method for detecting potassium dichromate by utilizing graphene quantum dot probe

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Embodiment Construction

[0017] In order to better understand the present invention, the present invention will be further elaborated below in conjunction with specific examples. It should be understood that the following examples are only some preferred implementations of the present invention, the purpose of which is to better illustrate the content of the present invention, but not to limit the protection scope of the present invention.

[0018] Utilize the method that graphene quantum dot probe detects potassium dichromate as:

[0019] The concentration of graphene quantum dots was fixed at 0.3 mg / mL, and the concentration of potassium dichromate was 0, 1×10 -5 mol / L, 1×10 -4 mol / L, 1×10 -3 mol / L, then the graphene quantum dots are mixed with potassium dichromate, left to stand for 1 minute, configured into four parts of standard solutions, and under the condition that the excitation wavelength is 345nm, the fluorescence intensity of the standard solutions is detected respectively to obtain The...

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Abstract

The invention discloses a method for detecting potassium dichromate by utilizing a graphene quantum dot probe. The method is characterized by comprising the following steps: (1) establishing a linear relationship: preparing a standard solution of graphene quantum dot and potassium dichromate solution, and obtaining the linear relation between the fluorescent intensity of the graphene quantum dot and the concentration of the potassium dichromate through the fluorescent spectra; (2) detecting: detecting the fluorescent intensity of the to-be-detected potassium dichromate solution, and determining the content of the potassium dichromate in the to-be-detected potassium dichromate solution according to the linear relation. The method is easy to operate, rapid in detection, high in sensitivity and good in selectivity, has the characteristics of high sensitivity and high selectivity when potassium dichromate in a mixed sample is detected and is promising in application prospect.

Description

technical field [0001] The invention belongs to the technical field of chemical detection, and in particular relates to a method for detecting potassium dichromate by using a graphene quantum dot probe. Background technique [0002] Potassium dichromate is a toxic and carcinogenic strong oxidizing agent, it is orange-red solid at room temperature. It is classified as a first-class carcinogen by the International Agency for Research on Cancer, and it is a strong oxidant, which is widely used in laboratories and industries. Potassium dichromate is mainly used in the chemical industry as the main raw material for the production of chromium salt products such as chromium trioxide; in the match industry, it is used as an oxidant for making matchheads; in the enamel industry, it is used to make enamel powder to make enamel green; It is used as a coloring agent in the industry; as a mordant in the printing and dyeing industry; as an oxidizing agent in the fragrance industry; in ad...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/64
Inventor 肖琦黄珊丘杭娜王鲁敏盛家荣苏炜朱发伟
Owner GUANGXI TEACHERS EDUCATION UNIV
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