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Preparation method of metal probe applicable to AFM (Atomic Force Microscope)

An atomic force microscope, metal probe technology, applied in the field of nano-scale sharp probe preparation, can solve the problems of high process requirements, difficult to obtain solutions, difficult to commercial production, etc., to achieve low noise, avoid negative effects, end-to-end sharp effect

Inactive Publication Date: 2014-10-01
XIAMEN UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented describes methods that improve the accuracy and efficiency of measuring tiny metals like Au nanoparticles. These small particles have unique characteristics - they allow them to absorb energy from incident radiation while transmitting signals through their surfaces. By applying voltage across these particles, changes occur when there're no absorption occurs. Using this process allows for precise measurements over long distances. Additionally, the inventors found that adding a special substances called hydrogen peroxide improves its effectiveness compared to other chemical agents commonly used during the production phase. Overall, these technical improvements result in improved precision and reliability in detecting minute quantities of noble metals.

Problems solved by technology

Technological Problem addressed in this patents relates to improving the performance of AFC probes due to their ability to create strong interactions without being affected by external forces like pressure waves. Current methods involve complicated processes involving multiple steps, leading to reduced accuracy and decreased reliabilities over time. Therefore, new ways to make AFO probes become increasingly useful in applications requiring both qualitative inspections at finer dimensions and quantitation capabilities.

Method used

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  • Preparation method of metal probe applicable to AFM (Atomic Force Microscope)
  • Preparation method of metal probe applicable to AFM (Atomic Force Microscope)
  • Preparation method of metal probe applicable to AFM (Atomic Force Microscope)

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Embodiment 1

[0039] The present invention will be described below by taking the production of AFM gold probes as an example.

[0040] (1) Electrochemical etching of gold wire

[0041] In this example, a gold wire (Alfa Aesar Company) with a diameter of 50 μm was used, which was ultrasonically cleaned in acetone before use. The etchant is concentrated hydrochloric acid+absolute ethanol with a volume ratio of 1:1. figure 2 For the etching scheme, the gold wire is used as the working electrode, and the gold ring is used as the counter electrode to form a two-electrode system. Apply a voltage of 2.2V with a DC power supply. After about 30 seconds, the part of the gold wire immersed in the etchant falls off, and the etching stops automatically. The obtained gold needle tip was rinsed with ultrapure water.

[0042] (2) Use a silicon wafer to flatten the gold wire near the end of the needle tip

[0043] The silicon wafer is a polished silicon wafer (Zhejiang Lijing Silicon Material Co., Ltd....

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Abstract

The invention relates to a preparation method of a metal probe applicable to an AFM (Atomic Force Microscope). The method has the advantages of low cost, high success rate, wide probe tip application range and the like. The preparation method comprises the main steps as follows: firstly, performing electrochemical etching on metal wires, so as to obtain a probe tip with a sharp tail end; secondly, flattening metal wires close to the tail end of the probe tip by adopting silicon wafers or polycrystal sapphire pieces, wherein the flattened part is used as a suspension arm of an AFM probe; thirdly, bending the tail end of the probe tip by a certain angle, wherein the bent part is used as the probe tip of the AFM probe; fourthly, pasting the suspension arm on a specific substrate by using glue. The method can be used for manufacturing a metal probe made of various materials such as gold and silver, the tail end of the metal probe is sharp, the conductivity is excellent, and the preparation method is applicable to the AFM, various electrical measurement technologies (like an electrostatic force microscope) based on the AFM and a tip-enhanced Raman spectroscopy technology based on the AFM, and the like.

Description

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Claims

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Application Information

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Owner XIAMEN UNIV
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