Vacuum brazing solder, preparation method and application thereof
A brazing solder and vacuum technology, applied in the direction of welding equipment, welding/cutting medium/material, welding medium, etc., can solve problems such as weak welding and fracture of welded parts
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preparation example Construction
[0014] The invention provides a kind of preparation method of vacuum brazing solder, and described preparation method comprises:
[0015] 1) The process of mixing nickel powder, water glass and water to prepare suspended solder;
[0016] 2) at 30-45 ° C, the process of mixing the suspended solder and sodium carboxymethyl cellulose to prepare vacuum brazing solder;
[0017] Wherein, relative to 100 parts by weight of nickel powder, the amount of water glass is 0.25-2.5 parts by weight, the amount of sodium carboxymethylcellulose is 0.9-3.8 parts by weight, and the amount of water is 12-26 parts by weight .
[0018] In the present invention, the nickel powder can be any commercially available nickel powder. In order to make the prepared vacuum brazing solder better weld the parts to be welded together firmly, preferably the nickel powder The particle size of the powder is 0.2-0.5mm.
[0019] Simultaneously, in the present invention, described water glass refers to pure compou...
Embodiment 1
[0029] 1) At 20°C, mix 100g of nickel powder, 1.5g of water glass and 18g of water for 40 minutes to prepare suspended solder;
[0030] 2) At 40° C., the above suspension solder and 2.5 g of sodium carboxymethylcellulose were mixed for 25 minutes to prepare vacuum brazing solder.
[0031] Wherein, the particle diameter of nickel powder is 0.3mm, the modulus of water glass is 2, and the degree of polymerization of sodium carboxymethyl cellulose is 500.
[0032] The vacuum brazing solder obtained above is coated on iron-chromium-aluminum and stainless steel, then the temperature is raised to 1070° C. for brazing, and then the temperature is lowered to 25° C. to obtain a brazed workpiece. The fracture strength of this brazed workpiece was 8.1 MPa.
Embodiment 2
[0034] 1) At 20°C, mix 100g of nickel powder, 0.25g of water glass and 12g of water for 30 minutes to prepare suspended solder;
[0035] 2) At 30° C., the above suspension solder and 0.9 g of sodium carboxymethyl cellulose were mixed for 20 minutes to prepare vacuum brazing solder.
[0036] Wherein, the particle diameter of nickel powder is 0.2mm, the modulus of water glass is 1, and the degree of polymerization of sodium carboxymethyl cellulose is 100.
[0037] The vacuum brazing solder obtained above is coated on iron-chromium-aluminum and stainless steel, then the temperature is raised to 1070° C. for brazing, and then the temperature is lowered to 25° C. to obtain a brazed workpiece. The fracture strength of this brazed workpiece was 7.8 MPa.
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