Traditional Chinese medicine preparation lumbus-strengthening kidney-tonifying pill detection method

A technology of Zhuangyaobushen pills and detection methods, applied in measuring devices, material analysis through optical means, instruments, etc., can solve problems such as not reflecting drugs, improve controllability, improve quality standards, ensure internal quality and The effect of curative effect

Inactive Publication Date: 2015-04-01
JINGFUKANG PHARMA GRP CHIFENG DANLONG PHARMA CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, the above-mentioned standards have the following problems: in the technical standards, there are still shortcomings such as content measurement items and identification items that do not reflect the index components of the internal quality of the drug. In order to improve the product quality of traditional Chinese medicine, it is necessary to improve the product quality standard

Method used

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  • Traditional Chinese medicine preparation lumbus-strengthening kidney-tonifying pill detection method
  • Traditional Chinese medicine preparation lumbus-strengthening kidney-tonifying pill detection method
  • Traditional Chinese medicine preparation lumbus-strengthening kidney-tonifying pill detection method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] Zhuangyao Bushen pill quality standard after the improvement of embodiment 1:

[0043] prescription:

[0044]

[0045]

[0046] Preparation method: crush the above twenty flavors into fine powder, sieve, mix well, add 15-30g of refined honey for every 100g of powder, add appropriate amount of water, make pellets, and dry to obtain.

[0047] Properties: This product is a black honeyed pill; sweet and slightly sour.

[0048] Identification: by Figure 1-1~1-6 can be seen.

[0049] (1) Take this product and observe under a microscope: the parenchyma is grayish brown to dark brown, the cells are shrunken, and those containing brown nuclei are rehmannia glutinosa, see Picture 1-1 . Starch grains are triangular oval or oblong, with a diameter of 24-40 μm, and the umbilicus is short-slit or herringbone-shaped, which is a yam, see Figure 1-2 . Irregular branched masses are colorless and dissolve in chloral hydrate test solution; hyphae are colorless or light brown,...

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Abstract

The invention discloses a traditional Chinese medicine preparation lumbus-strengthening kidney-tonifying pill detection method, according to the method, rehmannia glutinosa, yam, tuckahoe, schisandra, chrysanthemum and astragalus in a lumbus-strengthening kidney-tonifying pill can be microscopically identified, a radix angelicae sinensis referenee crude herb, ginsenoside Rg1, ginsenoside Re, ginsenoside Rb1, dipsacus asper saponin VI, astragaloside and deoxyschizandrin are used as reference substances, whether the lumbus-strengthening kidney-tonifying pill contains the radix angelicae sinensis ,ginseng, dipsacus asper, astragalus and schisandra can be identified by thin-layer chromatography; the dipsacus asper saponin VI content in the lumbus-strengthening kidney-tonifying pill preparation can be detected by HPLC, according to the detection method, the quantitative index is that the dipsacus asper saponin VI (C47H76O18) content in every 1g of the traditional Chinese medicine preparation lumbus-strengthening kidney-tonifying pill may not be less than 0.60mg, the controllability of quality standards of the traditional Chinese medicine preparation lumbus-strengthening kidney-tonifying pill can be improved to further ensure the product intrinsic quality and effect, so that the quality standard is more perfect, and the drug quality control level is improved.

Description

technical field [0001] The invention belongs to the technical field of Chinese patent medicines, and relates to a method for testing Chinese medicine preparation Zhuangyaobushen pills made from Chinese medicinal materials. Background technique [0002] Zhuangyao Bushen Pills are included in the Ministry of Health Drug Standards Chinese Medicine Prescriptions Volume II, the standard number is WS 3 -B-0273-90, record prescription and quality standard: [0003] prescription: [0004] [0005] However, the above-mentioned standards have the following problems: there are still shortcomings in the technical standards that do not reflect the content measurement items of the index components that reflect the internal quality of the drug, and the identification items. In order to improve the product quality of traditional Chinese medicine, it is necessary to improve the product quality standard. Contents of the invention [0006] The purpose of the present invention is to over...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/84G01N30/90G01N30/02
Inventor 李树庆董海荣李君周海英薛显丽张静
Owner JINGFUKANG PHARMA GRP CHIFENG DANLONG PHARMA CO LTD
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