IgM-rich human immunoglobulin preparation and preparation method thereof
A technology for human immunoglobulin and protein preparations, which is applied in the field of preparation of blood products, can solve the problems of allergies, separation difficulties, and large side effects in patients, and achieves the effects of low IgA content, high safety, and small side effects.
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Embodiment 1
[0036] Embodiment 1 uses the preparation of the immunoglobulin preparation rich in IgM of the present invention
[0037] 1. Experimental materials
[0038] Cohn fraction I+I+I or fraction I+I: prepared according to the low-temperature ethanol precipitation method described in "Medical Biological Products" (People's Health Publishing House), second edition, page 1194.
[0039] Hydrochloric acid, octanoic acid, CaptoQ filler, GigacapQ filler, UnosphereQ filler, MacrocapQ, diatomaceous earth and Beckman IMMAGE IgA detection kit are all commercially available.
[0040] 2. Experimental method
[0041] Flowchart such as figure 1 Shown:
[0042] 2.1 Separation and purification method:
[0043] Dissolve 4kg of component I+II+III precipitate in 40L of 5°C water for injection, stir for 1 hour, use 0.5M acetic acid to adjust the pH to 4.20, heat and stir in a 25°C water bath for 2 hours to increase the required IgG solubility and fully dissolve.
[0044] Add octanoic acid directly t...
Embodiment 2
[0057] Embodiment 2 uses the preparation of the immunoglobulin preparation rich in IgM of the present invention
[0058] 1. Experimental materials
[0059] Cohn fraction I+I+I or fraction I+I: prepared according to the low-temperature ethanol precipitation method described in "Medical Biological Products" (People's Health Publishing House), second edition, page 1194.
[0060] Hydrochloric acid, octanoic acid, CaptoQ filler, GigacapQ filler, UnosphereQ filler, MacrocapQ, diatomaceous earth and Beckman IMMAGE IgA detection kit are all commercially available.
[0061] 2. Experimental method
[0062] Flowchart such as figure 1 Shown:
[0063] 2.1 Separation and purification method:
[0064] Dissolve 4kg of component I+II+III precipitate in 40L of 5°C water for injection, stir for 1 hour, use 0.5M acetic acid to adjust the pH to 4.20, heat and stir in a 25°C water bath for 2 hours to increase the required IgG solubility and fully dissolve.
[0065] Add octanoic acid directly t...
Embodiment 3
[0078] Embodiment 3 uses the preparation of the immunoglobulin preparation rich in IgM of the present invention
[0079] 1. Experimental materials
[0080] Cohn fraction I+I+I or fraction I+I: prepared according to the low-temperature ethanol precipitation method described in "Medical Biological Products" (People's Health Publishing House), second edition, page 1194.
[0081] Glacial acetic acid, sodium octanoate, CaptoQ filler, GigacapQ filler, UnosphereQ filler, MacrocapQ, diatomaceous earth, and Beckman IMMAGE IgA detection kit are all commercially available.
[0082] 2. Experimental method
[0083] Flowchart such as figure 1 Shown:
[0084] 2.1 Separation and purification method:
[0085] Dissolve 4kg of component I+II+III precipitate in 40L of 5°C water for injection, stir for 1 hour, use 0.5M acetic acid to adjust the pH to 4.20, heat and stir in a 25°C water bath for 2 hours to increase the required IgG solubility and fully dissolve.
[0086] Add 1mol / L sodium octa...
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