High-viscosity curing agent composition
A technology of composition and curing agent, applied in the field of high-viscosity curing agent composition, can solve the problems of high cost, loss of marketization significance, insufficient bonding strength, etc.
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Embodiment 1
[0014] I. the synthesis of formula 1 compound
[0015]
Synthetic example
[0016] The compound described in Formula 1 is a known compound, which can be purchased commercially or prepared synthetically by those skilled in the art. Its typical but non-limiting synthetic examples are as follows:
[0017] A solution A in which 18.82 g of m-xylene diisocyanate was dissolved in 100 g of isopropanol, and a solution B in which 25.3 g of hydrazine was dissolved in 100 g of isopropanol were prepared. While stirring the solution B in the three-necked flask while controlling it at 30° C., the solution A was added dropwise at a rate of 1.4 g / min. After the dropwise addition of the solution A was completed, the reaction solution was measured with a Fourier transform infrared spectrophotometer, and it was confirmed that the 2250 cm from the isocyanate group -1 The reaction was terminated after the disappearance of the nearby peak. It reacted so that hydrazine may be 5 mol (1:5 by molar ratio) with respect to 1 mol of m-xylene diisocyanate.
[0018] After the rea...
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