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A kind of making method of commemorative diamond

A production method and diamond technology, applied to diamonds, measuring devices, instruments, etc., can solve problems such as low carbon purity and difficulty in meeting diamond production requirements, and achieve the effect of avoiding incomplete cremation

Active Publication Date: 2017-09-12
成都艾美可尔品牌管理有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In view of this, the present invention provides a method for making commemorative diamonds and a carbon-containing detection method for the obtained diamonds, so as to improve the low purity of carbon extracted from the bone-containing tissues of living organisms, which is difficult to meet the requirements of diamond production. asked questions

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  • A kind of making method of commemorative diamond
  • A kind of making method of commemorative diamond
  • A kind of making method of commemorative diamond

Examples

Experimental program
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Effect test

Embodiment 1

[0074] figure 1 The method for making commemorative diamonds provided by Embodiment 1 of the present invention is shown, and the sample tissue is selected from all the ashes of adults, including the following steps:

[0075] a. Grinding the ashes to a particle size of 10 μm to obtain 505 g of powder;

[0076] b. Dissolve the powder in a mixed solution of 50% sulfuric acid solution, 30% nitric acid solution, and 38% hydrochloric acid solution. The volume ratio of sulfuric acid solution, nitric acid solution, and hydrochloric acid solution is 2:1:1. Rotate at 100rpm and react for 30min, then filter, wash the crude carbon with distilled water, and adjust the pH of the crude carbon to 6;

[0077] c. Put the crude carbon product in an inner series graphitization furnace and purify it at 1800°C for 1.2h;

[0078] d. At 1200°C and 1200MPa, place all the extracted carbon on the side close to the Ni-Mn-Co catalyst and the diamond seed crystal for cultivation.

[0079] After the cult...

Embodiment 2

[0082] image 3 The manufacturing method of the commemorative diamond provided by the embodiment of the present invention two is shown, the sample tissue is selected animal body skin for use, comprises the following steps:

[0083] a. Put the animal skin into the dryer, blow in nitrogen, discharge the residual air in the dryer, dry the boneless tissue at 200°C until its water content is 25%, and then crush it to the particle size 20 μm, get 500g of powder, mix the powder with labeled carbon, pour the powder into 95% dehydrated alcohol by weight, stir constantly, then filter out the powder, and then use an organic element analyzer to analyze the powder Elemental analysis, the analysis shows that the powder contains 0.09% metal ions;

[0084] b. Put the powder into the oven, isolate the air, and vent the residual air in the oven with nitrogen and hydrogen. The volume of hydrogen accounts for 8% of the total volume of the gas, and then heat the powder to 800°C. Carry out the ca...

Embodiment 3

[0094] Figure 8 The manufacturing method of the commemorative diamond provided by the third embodiment of the present invention is shown, and the sample tissue is selected from all the ashes of children, including the following steps:

[0095] a. Grinding the ashes to a particle size of 18 μm to obtain 350 g of powder;

[0096] b. Dissolve the powder in a 50% by weight phosphoric acid solution, then pour the resulting mixture into a blender, process it for 60 minutes at a speed of 100rpm, then pour out the mixture, and mix it with 5% by weight of sodium hydroxide The solution undergoes a neutralization reaction, adjusts the pH value to 6, filters, and then uses distilled water to wash and filter the solid matter, then put the solid matter in a constant temperature drying oven, and dry it at 130°C for 30 minutes to obtain a crude carbon product;

[0097] c. Put the crude carbon obtained in an Acheson furnace and purify at 2500°C for 1 hour;

[0098] Put the purified carbon c...

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Abstract

The invention provides a memory diamond making method and relates to the technical field of diamond making. The memory diamond making method comprises the several steps of grinding, pickling, further purification and diamond cultivation. The purity of carbon extracted by means of the memory diamond making method is very high, additional carbon sources are fewer during diamond making, and resources are saved. The invention further provides a method for detecting the carbon content of made diamond. The method for detecting the carbon content can utilize labeled carbon to track carbon in sample tissues, the labeled carbon can track the whole purification process and more comprehensively prove that the carbon in the sample tissues is more reliable in use if the labeled carbon is mixed in powder, and the proportion of the carbon, retained in the memory diamond, of the sample tissues can be quantitatively identified through calculation if the labeled carbon mixed in a crude carbon product.

Description

technical field [0001] The invention relates to the technical field of making diamonds, in particular to a method for making commemorative diamonds. Background technique [0002] The deceased will be cremated, and the ashes after cremation become their only certificate, and also the spiritual sustenance for their family members and friends to remember the deceased. Based on the relatives' consideration for the deceased, in the existing technology, there is an operation of extracting the carbon from the ashes of the deceased obtained after cremation to make diamonds for their loved ones to wear, and then remembering the deceased, realizing spiritually, The wish of the dead to be with them. However, in the extraction operation in the prior art, in order to extract the carbon that meets the purity requirements of diamond cultivation, most of the dead are cremated in a low temperature area, and the cremation is not complete. For their relatives, this kind of operation is a kind...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B32/26G01N33/00
Inventor 刘逸舟戴乐德王健
Owner 成都艾美可尔品牌管理有限公司
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