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Preparation method of cigarette filter tip rod with blending material controlled-release cool sense essence

A cooling and flavoring technology, applied in the field of tobacco, can solve the problems of volatile cool taste, volatile flavor, and affect the taste, and achieve the effects of prolonging release time, long-lasting release performance and increasing storage time

Active Publication Date: 2016-06-22
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

With the continuous improvement of people's requirements for cool products, the shortcomings and deficiencies of menthol are gradually exposed, which are mainly manifested in two aspects. One is in terms of high temperature resistance. , especially the loss of aroma and fragrance in the product after high temperature is very large, which seriously affects the taste of the product
The second is that the duration of cool feeling of menthol in people's skin and oral cavity is shorter
[0004] Existing research shows that temperature-sensitive controlled-release technology is relatively mature in the field of medicine, but only this applicant has tried temperature-sensitive controlled-release technology in the tobacco industry, and applied for an invention patent in 2012. The invention patent The name of the patent is the preparation method of temperature-sensitive controlled-release flavoring drop pills for cigarettes (CN201210544175.X). Make temperature-sensitive smoking drop pills with a diameter of 3.6-4mm. The drop pill is a hard ball. Put the drop pill directly into the mouth stick. Since the drop pill is visible and tactile, it will It will affect the taste, and it cannot ensure the uniform distribution of cool taste
In addition, because the essence is easy to volatilize, the cool taste of general cool-feeling cigarettes is easy to volatilize during storage, and it is difficult to preserve

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A method for preparing a mouthpiece stick for cigarettes with controlled-release cooling essence of blended materials, characterized in that the specific steps are as follows:

[0027] (1) Weigh 100g of hydroxypropyl cyclodextrin, add 500g of water at a weight ratio of 1:5 (hydroxypropyl cyclodextrin: water), and stir at 30°C until the supramolecular material hydroxypropyl The cyclodextrin is completely dissolved to reach a clear and transparent state, and a supramolecular material solution is obtained;

[0028] (2) Weigh 100g of polyethylene glycol with a molecular weight of 5000, add 400g of 95% ethanol solution with a mass fraction of 95% in a weight ratio of 1:4 (polyethylene glycol: 95% aqueous ethanol solution), at 30°C Stir until the polyethylene glycol is completely dissolved to obtain a thermosensitive polymer solution;

[0029](3) Weigh 100 g of the supramolecular material solution prepared in step (1) and 200 g of the thermosensitive polymer solution prepare...

Embodiment 2

[0036] A method for preparing a mouthpiece stick for cigarettes with controlled-release cooling essence of blended materials, characterized in that the specific steps are as follows:

[0037] (1) Weigh 100g of aminoporphyrin, add 1kg of 20% ethanol solution by mass fraction in a ratio of 1:10 by weight (aminoporphyrin: 20% aqueous ethanol solution), and stir at 40°C until the supramolecular material Completely dissolve to reach a clear and transparent state, and obtain a supramolecular material solution;

[0038] (2) Weigh 100g of polyvinyl isobutyramide with a molecular weight of 10000, add 1kg of 50% ethanol aqueous solution at a weight ratio of 1:10 (polyvinyl isobutyramide: 50% ethanol aqueous solution), at 40°C Stir until the material is completely dissolved to obtain a temperature-sensitive polymer solution;

[0039] (3) Weigh 100 g of the supramolecular material solution prepared in step (1) and 500 g of the temperature-sensitive high-molecular material solution prepar...

Embodiment 3

[0046] A method for preparing a mouthpiece stick for cigarettes with controlled-release cooling essence of blended materials, characterized in that the specific steps are as follows:

[0047] (1) Take by weighing 100g of calixarene sulfonate sodium, add 1.5kg mass fraction of 60% ethanol aqueous solution at a weight ratio of 1:15 (calixarene sulfonate: 60% aqueous ethanol solution), at 50°C Stir until the supramolecular material is completely dissolved to obtain a supramolecular material solution;

[0048] (2) Weigh 200g of poloxamer with a molecular weight of 8000, add 2.4kg of aqueous solution in a ratio of 1:12 by weight (poloxamer: aqueous solution), and stir at 50°C until the material is completely dissolved to obtain a warm Sensitive polymer solution;

[0049] (3) Weigh 100 g of the supramolecular material solution prepared in step (1) and 800 g of the temperature-sensitive high-molecular material solution prepared in step (2) according to the ratio of 1:8 by weight of ...

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PUM

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Abstract

The invention provides a preparation method of a cigarette filter tip rod with blending material controlled-release cool sense essence. The preparation method comprises the specific steps that a supermolecular material and aqueous ethanol with the mass fraction of 0%-95% are mixed to be uniform according to the weight ratio of 1:0.5-1:30 to obtain a supermolecular solution; a temperature-sensitive macromolecular material and aqueous ethanol with the mass fraction of 0%-95% are mixed to be uniform according to the weight ratio of 1:0.5-1:30 to obtain a temperature-sensitive macromolecular solution; the supermolecular material solution and the temperature-sensitive macromolecular solution are mixed according to the weight ratio of 1:(0.1-10) and then subjected to ultrasonic treatment, a cool sense essence solution mixed with aqueous ethanol is added into the mixed solution, stirring is performed, the mixed solution is subjected to ultrasonic treatment and then applied to shreds in the filter tip rod forming process, and the cigarette filter tip rod is obtained after filter tip rod forming. According to the cigarette filter tip rod, essence is slowly and continuously released, therefore, the cigarette smoking comfort is improved, and harm of a cigarette to human health is reduced.

Description

technical field [0001] The invention belongs to the technical field of tobacco, and in particular relates to a method for preparing a mouthpiece for cigarettes with a controlled-release cooling flavor of blended materials. Background technique [0002] Because the cool essence is widely used in daily chemicals, food, tobacco, medicine and personal hygiene products, it has been paid attention to by people for a long time. Natural menthol is one of the most widely used spices in cool flavors. It is always favored by people because of its low price, pure taste, safety and easy availability. With the continuous improvement of people's requirements for cool products, the shortcomings and deficiencies of menthol are gradually exposed, which are mainly manifested in two aspects. One is in terms of high temperature resistance. , especially the loss of aroma and fragrance in the product after high temperature is very large, which seriously affects the taste of the product. The 2nd,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24D3/02A24D3/06
Inventor 王娜熊国玺司辉谢豪张耀华王萍庞哲张敦铁
Owner HUBEI CHINA TOBACCO IND
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