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An experimental method for studying the microscopic mechanism of material damage based on in-situ analysis technology

A technology of in-situ analysis and experimental method, which is applied in the analysis of materials, material analysis by radiation, and material analysis by optical means. Reproduce damage evolution and other issues

Active Publication Date: 2018-11-06
BEIJING INST OF STRUCTURE & ENVIRONMENT ENG +1
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  • Description
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Problems solved by technology

Although the post-analysis method can determine the initiation position of the crack on the fracture surface, it cannot reproduce the damage evolution process; although the surface in-situ observation test based on the scanning electron microscope can observe the dynamic evolution process of the crack on the surface, it can only The cracks on the surface are observed, and the relationship between the crack evolution and the mechanical field cannot be given, and the microscopic mechanism of damage cannot be revealed in depth

Method used

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  • An experimental method for studying the microscopic mechanism of material damage based on in-situ analysis technology
  • An experimental method for studying the microscopic mechanism of material damage based on in-situ analysis technology
  • An experimental method for studying the microscopic mechanism of material damage based on in-situ analysis technology

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Embodiment 2

[0046] Experimental approach to 2D in situ analysis techniques

[0047] (1) The 2D sample used is as image 3 shown. The surface of the 2D sample was ground, polished (~1 / 4 micron). The chemical erosion method is used to form "natural speckle" on the surface of the sample, so that the subsequent full-field measurement based on digital image correlation technology can achieve ideal accuracy without adding a layer of artificial spray speckle to the surface.

[0048] (2) The lost foam casting aluminum-silicon alloy contains a large number of casting defects (pores, shrinkage cavities, etc.), and the large-scale defects near the surface are most likely to become the crack initiation area. The casting defect in the notch area of ​​the sample was characterized by using a laboratory X-ray tomography device, so as to determine the next area to be observed.

[0049] (3) 2D in situ observation test device such as Figure 4 As shown, the fatigue loading is carried out by a standard h...

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Abstract

An experimental method for studying material damage micromechanism based on in-situ analysis includes an experimental method of 2D in-situ analysis and an experimental method of 3D in-situ analysis and includes the specific steps as follows: the experimental method of 2D in-situ analysis includes: preparing a sample, a plane sample, determining an in-situ observation area, and predicting a surface cracking area or presetting an artificial gap; performing in-situ online testing; analyzing damage micromechanism; the experimental method of 3D in-situ analysis includes: preparing a sample and selecting a 3D sample identical to the 2D sample in material; determining an in-situ observation area, predicting a cracking part in connection with the distribution of microscopic composition of internal defects and the like, and using as a subsequent in-situ observation area; performing in-situ online testing; analyzing damage micromechanism. The 3D in-situ analyze enables observation and measurement for damage evolution in three-dimensional space, the 2D in-situ analysis has higher resolution and enables real-time imaging observation, and the two experimental means may be combined to complement each other's advantages.

Description

technical field [0001] The invention belongs to the field of experimental solid mechanics, and in particular relates to an experimental method for studying the microscopic mechanism of material damage, which adopts 2D and 3D in-situ analysis techniques. Background technique [0002] The microscopic mechanism of material damage provides an important basis for the optimal design of material structure, the strength prediction and life prediction of materials and structures, so it is of great significance to reveal the microscopic mechanism of material damage. The traditional experimental research methods on the microscopic mechanism of material damage generally adopt the experimental method of post-analysis or in-situ surface observation based on scanning electron microscopy. Although the post-analysis method can determine the initiation position of the crack on the fracture surface, it cannot reproduce the damage evolution process; although the surface in-situ observation test...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N23/04G01N21/84
CPCG01N21/84G01N23/046
Inventor 王龙吴建国李海波宫文然孔凡金刘武刚冯国林李志强
Owner BEIJING INST OF STRUCTURE & ENVIRONMENT ENG
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