Ultrahigh-strength electrolytic copper foil, an electrode and a secondary battery comprising the same, and a method of manufacturing the same
A technology of electrolytic copper foil and secondary battery, which is applied in the field of electrolytic copper foil, and can solve problems such as production efficiency degradation and inherent advantage damage
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example 1
[0072] An electrical current is conducted between the spaced cathode plates and the rotating anode cylinder in the electrolyte in the electrolyte tank to form a copper film on the rotating anode cylinder. The electrolyte contains 85g / L copper ions and 98g / L sulfuric acid. The electrolyte solution included 5.6 ppm of [bis(3-sulfopropyl) disulfide] (SPS), 6.2 ppm of collagen A (average molecular weight: 3000 g / mol to 20000 g / mol) and 1.1 ppm of (H 2 N) 2 C=S. When forming the copper film, maintain the electrolyte at about 50°C, and 3 A flow rate of / h feeds the electrolyte into the electrolyte tank. The current density provided for the formation of copper film is 55A / dm 2 . The copper film was dipped in a 1 g / L to 10 g / L potassium dichromate solution at room temperature for 10 seconds, and then dried to form a protective layer on both surfaces of the copper film, thereby completing an electrolytic copper film having a thickness of 4 μm foil.
example 2
[0074] In addition to the (H 2 N(CH 2 ) 6 ) 2 C=S was added to the electrolyte in an amount of 1.1ppm to replace (H 2 N) 2 Electrolytic copper foil was produced in the same manner as in Example 1 except for C=S.
example 3
[0076] In addition to the (H 2 N) 2 Electrolytic copper foil was produced in the same manner as in Example 1 except that the amount of C=S was 6.4 ppm.
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Abstract
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