Butadiene selective hydrogenation catalyst
A technology for selective hydrogenation and butadiene, applied in physical/chemical process catalysts, metal/metal oxide/metal hydroxide catalysts, hydrogenation to hydrocarbons, etc., can solve problems such as poor selectivity, limited application and development
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Embodiment 1
[0035] 1. Catalyst preparation
[0036] Take by weighing 14 grams of pseudo-boehmite equivalent to 10 grams of alumina, 130 grams of alumina, and 9 grams of asparagus powder, mix, then add 20 grams of polyvinyl alcohol-containing solution (mass concentration is 5%), and the mass concentration is 3.0 grams of 68% nitric acid, 200 milliliters of water, squeezed into mm clover-shaped carrier, the wet strip was dried at 110°C for 4 hours and then calcined at 750°C for 4 hours to obtain carrier Z1. Mix 20 grams of the above-mentioned carrier with nickel nitrate-silver nitrate mixed aqueous solution 26 containing 14 grams of nickel and 2.0 grams of silver, dry at 110° C. for 8 hours, and calcinate at 550° C. for 4 hours to obtain a Ni-based catalyst. Restore with hydrogen for 4 hours before use, the reduction temperature is 450°C, and the volumetric space velocity of hydrogen is 50 hours -1 , to obtain a low isomerism, selective hydrogenation catalyst, the specific composition is...
Embodiment 2
[0046] 1. Catalyst preparation
[0047] Take by weighing 14 grams of pseudo-boehmite equivalent to 10 grams of alumina, 130 grams of alumina, and 9 grams of asparagus powder, mix, then add 20 grams of polyvinyl alcohol-containing solution (mass concentration is 5%), and the mass concentration is 3.0 grams of 68% nitric acid, 200 milliliters of water, squeezed into mm clover-shaped carrier, the wet strip was dried at 110°C for 4 hours and then calcined at 750°C for 4 hours to obtain carrier Z1. Mix 20 grams of the above carrier with 26 grams of nickel nitrate-silver nitrate mixed aqueous solution containing 14 grams of nickel and 2.0 grams of silver, dry at 110°C for 8 hours, and calcined at 550°C for 4 hours to prepare a Ni-based catalyst. Restore with hydrogen for 4 hours before use, the reduction temperature is 450°C, and the volumetric space velocity of hydrogen is 50 hours -1 , to obtain a low isomerism, selective hydrogenation catalyst, the specific composition is show...
Embodiment 3
[0057] 1. Catalyst preparation
[0058] Take by weighing 14 grams of pseudo-boehmite equivalent to 10 grams of alumina, 130 grams of alumina, and 9 grams of asparagus powder, mix, then add 20 grams of polyvinyl alcohol-containing solution (mass concentration is 5%), and the mass concentration is 3.0 grams of 68% nitric acid, 200 milliliters of water, squeezed into mm clover-shaped carrier, the wet strip was dried at 110°C for 4 hours and then calcined at 750°C for 4 hours to obtain carrier Z1. Mix 20 grams of the above-mentioned carrier with 26 grams of nickel nitrate-silver nitrate-auric acid mixed aqueous solution containing 14 grams of nickel, 1.0 grams of silver and 1.0 grams of gold, dry at 110°C for 8 hours, and bake at 550°C for 4 hours to prepare Obtain Ni-based catalyst. Restore with hydrogen for 4 hours before use, the reduction temperature is 450°C, and the volumetric space velocity of hydrogen is 50 hours -1 , to obtain a low isomerism, selective hydrogenation ...
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