A kind of silver-loaded expanded graphite prepared from extra large flake graphite and its preparation and application
A technology of expanded graphite and flake graphite, which is applied in the field of materials, can solve the problems that expanded graphite particles are easy to fall off and affect the use effect, and achieve the effect of low cost, good use effect and avoiding bacterial infection
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Embodiment 1
[0029] A preparation method of silver-loaded expanded graphite prepared from extra-large flake graphite, utilizing the impregnation reduction method, comprising the following steps
[0030] Step 1, using extra large flake graphite as raw material, adopting a chemical oxidation method to obtain expandable graphite.
[0031] Step 2, under magnetic stirring, in silver nitrate solution (silver nitrate concentration is 0.02mol / L), slowly add the ammoniacal liquor that mass fraction is 10%, after the precipitate that produces is dissolved, configure silver ammonia solution, take 0.5g can be Put expanded graphite into 70mL silver ammonia solution and stir at room temperature for 30min, add dropwise 7mL (concentration: 0.2mol / L) of glucose solution, continue to stir at room temperature for 3h, wash with ultrapure water until the filtrate does not contain silver, then filter, and then place in 100 ℃ oven for 2 hours to obtain silver-loaded expandable graphite.
[0032] Step 3, rapid e...
Embodiment 2
[0035] A preparation method of silver-loaded expanded graphite prepared from extra-large flake graphite, utilizing the impregnation reduction method, comprising the following steps
[0036] Step 1, using extra large flake graphite as raw material, adopting a chemical oxidation method to obtain expandable graphite.
[0037] Step 2, under magnetic stirring, in silver nitrate solution (silver nitrate concentration is 0.005mol / L), slowly add the ammoniacal liquor that mass fraction is 10%, after the precipitate that produces is dissolved, configure silver ammonia solution, take 0.5g can Put expanded graphite into 70mL silver ammonia solution and stir at room temperature for 30min, add dropwise 2mL (concentration: 0.2mol / L) of glucose solution, continue to stir at room temperature for 3h, wash with ultrapure water until the filtrate does not contain silver, filter, and then place in 100 ℃ oven for 2 hours to obtain silver-loaded expandable graphite.
[0038] Step 3, rapid expansio...
Embodiment 3
[0041] A preparation method of silver-loaded expanded graphite prepared from extra-large flake graphite, utilizing the impregnation reduction method, comprising the following steps
[0042] Step 1, using extra large flake graphite as raw material, adopting a chemical oxidation method to obtain expandable graphite.
[0043] Step 2, under magnetic stirring, in silver nitrate solution (silver nitrate concentration is 0.00125mol / L), slowly add the ammoniacal liquor that mass fraction is 10%, after the precipitate that produces is dissolved, configure silver-ammonia solution, take 0.5g can be Put expanded graphite into 70mL silver ammonia solution and stir at room temperature for 30min, add dropwise 500μL (concentration: 0.2mol / L) of glucose solution, continue to stir at room temperature for 4h, wash with ultrapure water until the filtrate does not contain silver, filter, and then place in 100 ℃ oven for 2 hours to obtain silver-loaded expandable graphite.
[0044] In step three, ...
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