Application of Aidi preparation in preparation of medicine for treating malignant trophoblastic tumor
A trophoblast, tumor drug technology, applied in anti-tumor drugs, drug combinations, drug delivery, etc., can solve the problems of high toxicity and side effects, poor prognosis and quality of life
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Embodiment 1
[0077]Example 1: Preparation of Aidi injection (low component)
[0078]Ingredients: Cantharidin 4g, Ginseng 200g, Astragalus 450g, Acanthopanax 900g
[0079]Preparation method: take Cantharidum medicinal material, crush, extract 5 times with 400ml 100% ethanol under heating and reflux, extraction time respectively: 2h, 1h, 0.5h, 0.5h, 0.5h, filter, medicine residue for use, and use 4% for extract Adjust the sodium hydroxide solution to pH 8-9, recover ethanol under reduced pressure, filter, dilute to 1000ml with water, adjust to pH 6-7 with 12% hydrochloric acid solution, let stand, refrigerate, centrifuge and filter, supernatant with 4% hydrogen Adjust the sodium oxide solution to pH 8-9, ready for use; take ginseng slices, heat reflux with 480ml of 60% ethanol, extract for 3h, filter, and reserve for use. The extract is decompressed to recover the ethanol, and the concentrate is added with water to a volume of 150ml, and the hole is topped. Adsorption resin, add water to elute 5 times t...
Embodiment 2
[0080]Example 2: Preparation of Aidi injection
[0081]Ingredients: Cantharidin 5g, Ginseng 250g, Astragalus 500g, Acanthopanax 1000g
[0082]Preparation method: take Cantharidum medicinal material, crush, extract 5 times with 400ml 100% ethanol under heating and reflux, extraction time respectively: 2h, 1h, 0.5h, 0.5h, 0.5h, filter, medicine residue for use, and use 4% for extract Adjust the sodium hydroxide solution to pH 8-9, recover ethanol under reduced pressure, filter, dilute to 1000ml with water, adjust to pH 6-7 with 12% hydrochloric acid solution, let stand, refrigerate, centrifuge and filter, supernatant with 4% hydrogen Adjust the sodium oxide solution to pH 8-9, ready for use; take ginseng slices, heat reflux with 480ml of 60% ethanol, extract for 3h, filter, and reserve for use. The extract is decompressed to recover the ethanol, and the concentrate is added with water to a volume of 150ml, and the hole is topped. Adsorption resin, add water to elute 5 times the column volum...
Embodiment 3
[0083]Example 3: Preparation of Aidi injection
[0084]Ingredients: Cantharidin 10g, Ginseng 300g, Astragalus 750g, Acanthopanax 1250g
[0085]Preparation method: take Cantharidum medicinal material, crush, extract 5 times with 400ml 100% ethanol under heating and reflux, extraction time respectively: 2h, 1h, 0.5h, 0.5h, 0.5h, filter, medicine residue for use, and use 4% for extract Adjust the sodium hydroxide solution to pH 8-9, recover ethanol under reduced pressure, filter, dilute to 1000ml with water, adjust to pH 6-7 with 12% hydrochloric acid solution, let stand, refrigerate, centrifuge and filter, supernatant with 4% hydrogen Adjust the sodium oxide solution to pH 8-9, ready for use; take ginseng slices, heat reflux with 480ml of 60% ethanol, extract for 3h, filter, and reserve for use. The extract is decompressed to recover the ethanol, and the concentrate is added with water to a volume of 150ml, and the hole is topped. Adsorption resin, add water to elute 5 times the column volu...
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