Organic electrosynthesis electrolysis device

Abstract

The invention discloses an electrolysis device for organic electrosynthesis. The electrolysis cell is coaxially fixed on the body of a magnetic stirrer, the cover body covers the opening position of the electrolysis cell, and the inside of the side wall and the bottom wall of the electrolysis cell are provided with interconnected Interlayer, the interlayer is filled with thermal fluid; wherein, the center position of the bottom of the cover is fixed with a fixed plate, the electrode mechanism is fixed on the fixed plate, the wire harness for electrically connecting the electrode mechanism is set through the cover, and the top of the interlayer is set with Liquid inlet and exhaust port, the inner bottom of the electrolytic cell is provided with a magnet that matches the body of the magnetic stirrer; the external of the electrolytic cell is provided with a constant temperature heating device, and the constant temperature heating device is provided with an electric heating tube and a thermal resistor, and the electric heating tube Both the thermal resistance and the thermal resistance extend from the outer wall of the electrolytic tank into the heat conducting liquid and are sealed and fixed on the electrolytic tank, and the thermometer penetrates the cover and penetrates into the electrolytic tank. The organic electrosynthesis electrolysis device can provide a constant temperature electrolysis environment and stir the electrolytic solution.

Description

technical field [0001] The invention relates to laboratory equipment, in particular to an electrolysis device for organic electrosynthesis. Background technique [0002] Organic electrochemical synthesis technology is widely used in various fields of the national economy. Compared with conventional chemical synthesis methods, it has the advantages of high product purity, less environmental pollution, short process flow, and can be operated at normal pressure and temperature. It is a high-efficiency , highly selective synthetic method. [0003] Laboratory studies of organic electrochemical synthesis techniques usually use small electrolyzers as containers for organic electrochemical reactions. There are some disadvantages in the commonly used electrolytic cell, such as the electrolytic cell is open and cannot be completely sealed, and the reaction solution is exposed to the air; the electrolytic cell does not have a corresponding gas circuit, and the solution cannot be venti...

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Problems solved by technology

There are some disadvantages in the commonly used electrolytic cell, such as the electrolytic cell is open and cannot be completely sealed, and the reaction solution is exposed to the air; the electrolytic cell does not have a corresponding gas circuit, and the solution cannot be ventilated during the experiment; the design of the electrolytic cell is not good. Reasonable, the structure of the tank is complex; the distance between the electrodes is fixed and difficult to adjust; the solution in the electrolytic tank cannot react under constant temperature conditions, the reaction process cannot be stirred, and the electrolysis efficiency is low

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