li 8 narb 3 (so 4 ) 6 ·2h 2 oCompounds, nonlinear optical crystals and their preparation methods and uses
A 6·2H2O, nonlinear optics technology, applied in nonlinear optics, rubidium/cesium/francium compounds, alkali metal compounds, etc., can solve the problem of inability to achieve 1064nm wavelength laser quadruple frequency output, limiting output power and beam quality, It is difficult to achieve commercial application and other problems, and achieve the effect of short UV absorption cut-off edge, low cost, and large nonlinear optical effect.
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Embodiment 1
[0030] Adopt aqueous solution method, reaction equation is as follows:
[0031] 8Li 2 SO4·H 2 O+Na 2 SO 4 +3Rb 2 SO 4 =2Li 8 NaRb 3 (SO 4 ) 6 2H 2 O+4H 2 o
[0032] The specific operation steps are:
[0033] a. Will Li 2 SO4 H2O, Na 2 SO4, Rb 2 Weigh SO4 at a molar ratio of 8(10.234g):1(1.420g):3(8.010g) and put it into a clean beaker (clean the beaker with acid first, then rinse it with deionized water), add 60ml of deionized water, then ultrasonic treatment for 10 minutes to make it fully mixed and dissolved;
[0034] b. Seal the beaker containing the solution in step a with plastic wrap and place it in a static environment without shaking, pollution, and air convection. Prick the seal with several small holes to adjust the evaporation rate of water in the aqueous solution. Stand at low temperature (30°C-70°C) for 15-30 days;
[0035] c. Treat the solution in step b to grow crystal particles at the bottom of the beaker until the size of the crystal particle...
Embodiment 2
[0038] Adopt aqueous solution method, reaction equation is as follows:
[0039] 8Li 2 SO4·H 2 O+Na 2 SO 4 10H 2 O+3Rb 2 SO 4 =2Li 8 NaRb 3 (SO 4 ) 6 2H 2 O+14H 2 o
[0040] The specific operation steps are:
[0041] a. Will Li 2 SO4 H2O, Na 2 SO4·10H 2 O, Rb 2 SO4 was weighed at a molar ratio of 8(10.234g):1(3.222g):3(8.010g) and put into a clean beaker (the beaker must be cleaned with acid first, and then rinsed with deionized water), and added 60ml of deionized water, then ultrasonic treatment for 10 minutes to make it fully mixed and dissolved;
[0042] b. Seal the beaker containing the solution in step a with plastic wrap and place it in a static environment without shaking, pollution, and air convection. Prick the seal with several small holes to adjust the evaporation rate of water in the aqueous solution. Stand at low temperature (30°C-70°C) for 15-30 days;
[0043] c. Treat the solution in step b to grow crystal particles at the bottom of the beaker...
Embodiment 3
[0046] Adopt aqueous solution method, reaction equation is as follows:
[0047] 8Li 2 SO4+Na 2 SO 4 +3Rb 2 SO 4 +4H 2 O=2Li 8 NaRb 3 (SO 4 ) 6 2H 2 o
[0048] The specific operation steps are:
[0049] a. Will Li 2 SO4, Na 2 SO4, Rb 2 Weigh SO4 at a molar ratio of 8(8.795g):1(1.420g):3(8.010g) and put it into a clean beaker (clean the beaker with acid first, then rinse it with deionized water), add 60ml of deionized water, then ultrasonic treatment for 10 minutes to make it fully mixed and dissolved;
[0050] b. Seal the beaker containing the solution in step a with plastic wrap and place it in a static environment without shaking, pollution, and air convection. Prick the seal with several small holes to adjust the evaporation rate of water in the aqueous solution. Stand at low temperature (30°C-70°C) for 15-30 days;
[0051] c. Treat the solution in step b to grow crystal particles at the bottom of the beaker until the size of the crystal particles no longer ...
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