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Column plate structure capable of eliminating gas-phase deflected flow and design method

A technology of structural design and trays, applied in the field of chemical vapor-liquid mass transfer separation equipment, can solve the problems of reduced tray efficiency, induced trays, and pouring at the entrance of trays, etc., to eliminate liquid level drop and gas phase distribution. Uniform, uniform gas phase flow effect

Active Publication Date: 2019-01-15
CHANGZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Once the gas phase drift occurs, a large amount of gas phase flows out from the outlet of the tray, causing a large amount of mist entrainment; secondly, there is no or only a small amount of gas phase passing through the inlet of the tray, resulting in leakage at the inlet of the tray
This abnormal hydraulic phenomenon will not only significantly reduce the tray efficiency, but even induce tray flooding, affecting the normal operation of the column.
At present, some technologies such as multi-overflow trays, multi-downcomer trays and guided tray technologies can control the gas phase drift, but these technologies still have shortcomings: multi-overflow tray technology has complex design, especially with the increase of overflow number. There are disadvantages such as increase and long installation time; the efficiency of multi-downcomer trays is low; the technology of guided trays cannot cope with the conditions of high liquid / vapor ratio or lower limit operation of the distillation column

Method used

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  • Column plate structure capable of eliminating gas-phase deflected flow and design method
  • Column plate structure capable of eliminating gas-phase deflected flow and design method
  • Column plate structure capable of eliminating gas-phase deflected flow and design method

Examples

Experimental program
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Effect test

Embodiment 1

[0111] The design gas phase mass flow rate is 15000kg / hr, and the gas phase density is 2.5kg / m 3 , the mass flow rate of the liquid phase is 40000kg / hr, and the density of the liquid phase is 880kg / m 3 , the surface tension is 10N / m, and the viscosity is 1mPa·s. The mass transfer tray type is selected as a sieve tray column. Through the preliminary design, the structural parameters of the tray type are shown in Table 1:

[0112] Table 1 Design parameters of mass transfer tray structure

[0113]

[0114] The parameters calculated by formulas (1) to (9) are shown in Table 2:

[0115] Table 2 Calculation results of parameters related to the liquid level gradient of the mass transfer tray

[0116]

[0117] Divide the gas phase distribution plate into five zones, the length of each zone is 200 mm, and the ratio coefficient of gas phase distribution plate opening ratio is 1.4 (the gas phase distribution plate opening rate is 17.85%), then the gas phase distribution plate calc...

Embodiment 2

[0124] The design gas phase mass flow rate is 60000kg / hr, and the gas phase density is 2.5kg / m 3 , the mass flow rate of the liquid phase is 70000kg / hr, and the density of the liquid phase is 880kg / m 3 , the surface tension is 10N / m, and the viscosity is 1mPa·s. The mass transfer tray type is selected as a sieve tray column. Through the preliminary design, the structural parameters of the tray type are shown in Table 5:

[0125] Table 5 Mass transfer tray structure design parameters

[0126]

[0127] The parameters calculated by formulas (1) to (9) are shown in Table 6:

[0128] Table 6 Calculation results of parameters related to the liquid level gradient of the mass transfer tray

[0129]

[0130] The gas phase distribution plate is divided into four zones, the length of each zone is 400 mm, and the ratio coefficient of the gas phase distribution plate opening ratio is 1.4 (the gas phase distribution plate opening rate is 20.31%), then the gas phase distribution cal...

Embodiment 3

[0137] The design gas phase mass flow rate is 60000kg / hr, and the gas phase density is 2.5kg / m 3 , the mass flow rate of the liquid phase is 70000kg / hr, and the density of the liquid phase is 880kg / m 3 , the surface tension is 10N / m, and the viscosity is 1mPa·s. The mass transfer tray type is selected as a sieve tray column. Through the preliminary design, the structural parameters of the tray type are shown in Table 9:

[0138] Table 9 Mass transfer tray structure design parameters

[0139]

[0140] The parameters calculated by formulas (1) to (9) are shown in Table 10:

[0141] Table 10 Calculation results of parameters related to the liquid level gradient of the mass transfer tray

[0142]

[0143] Divide the gas phase distribution plate into two zones, the length of each zone is 800 mm, and the ratio coefficient of the opening ratio of the gas phase distribution plate is 1.4 (the opening rate of the gas phase distribution plate is 20.31%), then the gas phase distr...

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Abstract

The invention discloses a column plate structure capable of eliminating gas-phase deflected flow and a design method. The structure includes a mass transfer column plate, wherein a gas phase distribution plate is added to below the mass transfer column plate, thus forming a double-layer column plate structure. The distance from the gas phase distribution plate to the mass transfer column plate is20-300 mm. The gas phase distribution plate includes a non-holed zone, at one side, and a holed zone being the area except the non-holed zone. Horizontal baffles are formed on the holed zone of the gas phase distribution plate to separate the space, formed by the gas phase distribution plate and the mass transfer column plate, into several zones, wherein valve holes, in different numbers, are formed uniformly in each zones on the gas phase distribution plate, but the ratio of pore area of each zone to the area of each zone is equal. A part of the valve holes are provided with float valves. Thecolumn plate structure is simple and can effectively eliminate the forming condition of the gas-phase deflected flow and make gas-phase flow uniform. The structure greatly improves operating flexibility and separation efficiency.

Description

technical field [0001] The invention relates to a tray structure and a design method for eliminating gas-phase bias flow, and belongs to the technical field of chemical gas-liquid mass transfer separation equipment. Background technique [0002] At present, although a variety of new separation technologies have emerged, rectification is still the most widely used separation technology in industry. Among them, the most widely used is the rectification operation mode carried out by plate column. When the liquid phase flows on the tray, due to the influence of frictional resistance, the liquid layer on the tray will form a liquid level drop, resulting in uneven distribution of the liquid phase on the tray, and then forming a gas phase bias flow on the tray, especially on large-scale tray towers. . Once the gas phase drift occurs, a large amount of gas phase flows out from the outlet of the tray, causing a large amount of mist entrainment; secondly, no or only a small amount o...

Claims

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Application Information

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IPC IPC(8): B01D3/14B01D3/32
CPCB01D3/14B01D3/324
Inventor 王俊周鑫韶晖冷一欣黄春香孙雪妮
Owner CHANGZHOU UNIV
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