Shampoo comprising rose essential oil microcapsule and preparation method thereof
A technology of rose essential oil and hair shampoo, which is applied in the field of daily chemicals, can solve the problems of affecting product quality, short fragrance retention time, poor stability, etc., and achieve the effect of good embedding effect, high particle size uniformity, and high stability
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Embodiment 1
[0044] A preparation method of rose essential oil microcapsules, the concrete steps are:
[0045] Step 1): Dissolve 10.00g of β-cyclodextrin in 80mL of deionized water to obtain an aqueous solution of β-cyclodextrin, stir it in a water bath at 80°C to dissolve it, and obtain an aqueous solution of β-cyclodextrin, cool to 50°C and keep it warm spare;
[0046] Step 2): dissolving 2 g of rose essential oil in an organic solvent to obtain a rose essential oil solution; the organic solvent is absolute ethanol, and the volume ratio of rose essential oil to absolute ethanol is 1:20;
[0047] Step 3): Add the obtained rose essential oil solution into the β-cyclodextrin aqueous solution drop by drop at a uniform speed, and stir while adding, the β-cyclodextrin contained in the β-cyclodextrin aqueous solution and the rose essential oil solution contained The mass ratio of rose essential oil is 5:1, and the reaction solution is taken out after sealing and embedding in the dark at 50°C f...
Embodiment 2
[0060] Embodiment 2 (sustained release, stability experiment)
[0061] The rose essential oil microcapsules, the test of the slow-release effect under exposure to the air, the specific data of the time and the quality of the fragrance change are as follows figure 2 shown. The experimental results can prove that the overall particle size uniformity of the rose essence microcapsules is high, the mechanical strength is good, and the stability is strong.
Embodiment 3-5
[0063] A shampoo containing rose essential oil microcapsules, calculated by mass percentage, its composition and content are as follows:
[0064] Table 1 Rose-flavored shampoo formula table
[0065]
[0066]
[0067] The preparation method of the above-mentioned shampoo containing rose essential oil microcapsules is:
[0068] 1) Weigh the amount of each component, first add deionized water into the reaction kettle, stir and heat up to 60°C;
[0069] 2) Add preservatives and pearlescent agents to the deionized water in the reaction kettle in step 1), stir and dissolve, and prepare JR-400 aqueous solution (0.1% JR-400 and 9.9% water);
[0070] 3) Add AES, 6501, ammonium oxide and JR-400 aqueous solution to the reactor in step 2) and stir to dissolve;
[0071] 4) Finally add menthol to the reaction kettle in step 3), stir and dissolve, add citric acid to adjust the pH value of the solution to 5.5-6;
[0072] 5) Decrease the reaction kettle to room temperature, add rose e...
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