Shampoo containing citron essential oil microcapsules and preparation method of shampoo
A technology for shampoo and citron essential oil, applied in the field of daily chemicals, can solve the problems of affecting product quality, application effect, short fragrance retention time, etc., and achieves good embedding effect, strong stability and high particle size uniformity. Effect
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Embodiment 1
[0043] This example provides a kind of extracting method of citron essential oil, concrete steps are:
[0044] Step 1): Peel off the peel of the fresh citron fruit to remove the white fiber, and weigh 100g of the peel. (Try not to squeeze the oil sac)
[0045] Step 2): Weigh 0.3 g of calcium bicarbonate (the amount of calcium bicarbonate added is 0.3% of the weight of the peel), add water (the amount of water added is four times the weight of the peel, unit ml) and soak for 30-40 min.
[0046] Step 3): The soaked peel will become relatively brittle. After washing and washing away the calcium hydroxide, squeeze it with a Joyoung original juice machine, add 0.15% sodium chloride to the peel slurry, stir evenly and let it settle.
[0047] Step 4): Oil flakes can be seen floating on the liquid after 5 minutes, collect the oil flakes into a 45mL centrifuge tube, balance, and centrifuge at 9000r / min for 15min.
[0048] Step 5): Collect the essential oil after centrifugation, add a...
Embodiment 2
[0050] The present embodiment provides a kind of preparation method of citron essential oil microcapsules, and concrete steps are:
[0051] Step 1): Dissolve 10.00g of β-cyclodextrin in 80mL of deionized water to obtain an aqueous solution of β-cyclodextrin, stir it in a water bath at 80°C to dissolve it, and obtain an aqueous solution of β-cyclodextrin, cool to 50°C and keep it warm spare;
[0052] Step 2): the citron essential oil prepared by 2g embodiment 1 is dissolved in an organic solvent to obtain a citron essential oil solution; the organic solvent is dehydrated alcohol, and the volume ratio of the citron essential oil to dehydrated alcohol is 1: 20;
[0053] Step 3): Add the obtained citron essential oil solution to the β-cyclodextrin aqueous solution drop by drop at a constant speed, and stir while adding, and the β-cyclodextrin contained in the β-cyclodextrin aqueous solution and the citron essential oil solution The mass ratio of the citron essential oil containe...
Embodiment 3
[0066] Embodiment 3 (sustained release, stability experiment)
[0067] The citron essential oil microcapsules, the test of the slow-release effect under exposure to air, the specific data of the time and the change of the fragrance quality are as follows figure 2 shown. The experimental results can prove that the citron essence microcapsules have high overall particle size uniformity, good mechanical strength and strong stability.
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