Method for determining concentration of carbamazepine in plasma by liquid chromatography mass spectrometry
A technology of carbamazepine and LC/MS, applied in the field of medicine, can solve the problems such as the need to improve the accuracy and sensitivity, the health hazards of operators, and the import cost of reagents, etc., and achieve high sensitivity, simple pretreatment method, and stable baseline. Effect
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[0032] Example: Human K 2 Determination of Carbamazepine Concentration in EDTA Plasma
[0033] 1. Experimental materials and analytical equipment
[0034] Carbamazepine (analyte): Toronto Research Chemicals or equivalent or higher grade standard
[0035] Oxybutynin (internal standard): Toronto Research Chemicals or equivalent or higher grade standard
[0036] The reagents used are shown in Table 1 below:
[0037] Table 1 Reagent Details
[0038] Reagent name
level
manufacturer
HPLC
J. T. Baker
ACS
Adamas
[0039] Note: Reagents of the same grade or higher can also be used
[0040] The analytical equipment used is shown in Table 2 below:
[0041] Table 2 Details of equipment used
[0042] components
type
manufacturer
Binary pump (binary pump)
AC Pump
AB SCIEX
AB SCIEX
Column oven
AC Column oven
AB SCIEX
Autosa...
PUM
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