Preparation method of aquaculture nutrient water-regulating agent
An aquaculture and water agent technology, which is applied in chemical instruments and methods, biological water/sewage treatment, water/sludge/sewage treatment, etc. The effect of loosening air permeability, improving photosynthesis ability, and reducing ammonia nitrogen
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Embodiment 1
[0032] A kind of preparation method of aquaculture nutrient water-adjusting agent, prepares the water-adjusting agent by mixing and fermenting the mixed material containing compound microbial bacterial agent and titanium dioxide; The preparation method comprises the following steps:
[0033] 1) Preparation of Ag / TNTs;
[0034] Nano TiO 2After mixing the raw material and NaOH solution uniformly according to the ratio of material to liquid 1:30 (g / mL), move it into a polytetrafluoroethylene-lined autoclave, seal it, place it in an oven, and heat it at 80°C for 20 hours; then cool the product to room temperature, washed with deionized water until neutral, then added HCl solution, ultrasonically dispersed for 2 minutes, washed with deionized water until neutral, filtered and dried in an oven at 50°C, and the product was sealed and stored in a desiccator; among them, the concentration of NaOH solution 5mol·L -1 ;The concentration of HCl solution is 0.05mol L-1;
[0035] Place th...
Embodiment 2
[0046] A kind of preparation method of aquaculture nutrient water-adjusting agent, prepares the water-adjusting agent by mixing and fermenting the mixed material containing compound microbial bacterial agent and titanium dioxide; The preparation method comprises the following steps:
[0047] 1) Preparation of Ag / TNTs;
[0048] Nano TiO 2 After mixing the raw material and NaOH solution uniformly according to the ratio of material to liquid 1:42 (g / mL), move it into a polytetrafluoroethylene-lined autoclave, seal it, place it in an oven, and heat it at 115°C for 22 hours; then cool the product to room temperature, washed with deionized water until neutral, then added HCl solution, ultrasonically dispersed for 3 minutes, washed with deionized water until neutral, filtered and dried in an oven at 60°C, and the product was sealed and stored in a desiccator; among them, the concentration of NaOH solution 10mol·L -1 ; The concentration of HCl solution is 0.1mol L-1;
[0049] Place...
Embodiment 3
[0055] A kind of preparation method of aquaculture nutrient water-adjusting agent, prepares the water-adjusting agent by mixing and fermenting the mixed material containing compound microbial bacterial agent and titanium dioxide; The preparation method comprises the following steps:
[0056] 1) Preparation of Ag / TNTs;
[0057] Nano TiO 2 After mixing the raw material and NaOH solution uniformly according to the ratio of material to liquid 1:45 (g / mL), move it into a polytetrafluoroethylene-lined autoclave, seal it and put it in an oven, heat it at 130°C for 24h; then cool the product to room temperature, washed with deionized water until neutral, then added HCl solution, ultrasonically dispersed for 5 minutes, washed with deionized water until neutral, filtered and dried in an oven at 60°C, and the product was sealed and stored in a desiccator; among them, the concentration of NaOH solution 12mol·L -1 ; The concentration of HCl solution is 0.2mol L-1;
[0058] Place the pre...
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