A preparation method of high melting point resin powder material for selective laser sintering
A resin powder and laser sintering technology, which is applied in the field of additive manufacturing, can solve problems such as powder coating cracking, affecting the molding process, and sintering failure
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Embodiment 1
[0027] (1) Mix 1000g of PET resin powder with a particle size range of 30-100μm and 20g of silicon dioxide with a particle size of 20nm after polydimethylsiloxane treatment on the surface at a stirring rate of 1400r / min to obtain a PET powder predispersion , and then the above-mentioned powder predispersion, the remaining 3000g PET powder with a particle size range of 30-100μm, 8g N, N'-bis(3,5-di-tert-butyl-4-hydroxyphenylpropionamide), 4g2, 2'-Ethylene bis(4,6-di-tert-butylphenyl) fluorophosphite was added to a mixer, mixed evenly at a speed of 300r / min, and sieved to obtain PET powder material;
[0028] (2) The above-mentioned powders were sintered on selective laser sintering equipment. The parameters of the powder materials and sintering phenomena are shown in Table 1. The performance tests of the obtained sintered strips are shown in Table 2.
Embodiment 2
[0033] (1) Mix 1000g of PEI resin powder with a particle size range of 30-100μm and 20g of silicon dioxide with a particle size of 20nm treated by hexamethyldisilazane on the surface at a stirring rate of 1400r / min to obtain a PEI powder predispersion , and then the above-mentioned powder predispersion, the remaining 3000g of PEI powder with a particle size range of 30-100μm, 40g of 2,4-dihydroxybenzophenone, 8g of 2,6-di-tert-butyl-4-methyl-phenol, 4g2 , 2'-ethylenebis(4,6-di-tert-butylphenyl) fluorophosphite was added to the mixer, mixed evenly at a speed of 300r / min, and sieved to obtain PEI powder material;
[0034] (2) The above powder was sintered on Hunan Farsoon Hi-Tech ST252 selective laser sintering equipment. The powder material parameters and sintering phenomenon are shown in Table 1. The performance test of the obtained sintered sample is shown in Table 2.
Embodiment 3
[0039] (1) Mix 1000g of PPS resin powder with a particle size range of 30-100μm and 20g of silicon dioxide with a particle size of 20nm treated by hexamethyldisilazane on the surface at a stirring rate of 1400r / min to obtain a PPS powder predispersion , and then the above-mentioned powder predispersion, the remaining 3000g PPS powder with a particle size range of 30-100μm, 40g2,4-dihydroxybenzophenone, 8g2,6-di-tert-butyl-4-methyl-phenol, 4g2 , 2'-ethylenebis(4,6-di-tert-butylphenyl) fluorophosphite was added to the mixer, mixed evenly at a speed of 300r / min, and sieved to obtain the PPS powder material;
[0040] (2) The above powder was sintered on Hunan Farsoon Hi-Tech ST252 selective laser sintering equipment. The powder material parameters and sintering phenomenon are shown in Table 1. The performance test of the obtained sintered sample is shown in Table 2.
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