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A kind of quality detection method of Shuyanqing spray

A quality inspection method and spray technology, applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of poor accuracy of inspection results, and achieve the effect of improving accuracy and stabilizing product quality

Active Publication Date: 2022-07-01
GUILIN SANJIN PHARMACEUTICALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The technical problem to be solved by the present invention is to overcome the deficiencies of the prior art, and provide a quality detection method of Shuyanqing spray, so as to solve the technical problem of poor accuracy of the detection results simply applying the existing method

Method used

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  • A kind of quality detection method of Shuyanqing spray
  • A kind of quality detection method of Shuyanqing spray
  • A kind of quality detection method of Shuyanqing spray

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] The preparation of embodiment one Shuyanqing spray

[0045] The raw materials are as follows:

[0046] Watermelon Cream 40g, Scutellaria baicalensis 150g, Shegan 150g, Mountain Bean Root 100g, Shan Yinhua 160g, Fangfeng 80g, Menthol 3g, Borneol 2g, Borax 25g, Scrophularia 80g, Ophiopogon 80g, Licorice 80g

[0047] The preparation method is as follows:

[0048] The above twelve flavors, Shan Yinhua and Fangfeng are distilled with water, and about 200ml of distillate is collected. The distilled water solution is filtered and collected in another device; the medicinal residues are mixed with Scutellaria baicalensis, Shegan, Shandou root, Scrophulariaceae, Ophiopogon japonicus, and licorice root. Wait for the six flavors, add water for three times, 1 hour each time, combine the decoction, filter, combine the filtrate with the above distilled aqueous solution, concentrate to a relative density of 1.15-1.17 (60°C), add 85% ethanol to make the alcohol content When it reaches...

Embodiment 2

[0049] Example 2 Quality inspection of Shuyanqing spray

[0050] (1) Take 20ml of Shuyanqing spray, shake and extract 2 times with ethyl acetate, 20ml of ethyl acetate each time, wherein the ethyl acetate layer is discarded during shaking and extraction, and the water layer is retained; the water layer is saturated with water The n-butanol solution was shaken and extracted twice, each time the water-saturated n-butanol solution was 20ml, wherein, the water layer was discarded during the shaking extraction, the n-butanol layer was retained, and the combined n-butanol layer; n-butanol layer; Shake and extract twice with a saturated aqueous solution of n-butanol, each time 20 ml of a saturated aqueous solution of n-butanol, divide the n-butanol solution, evaporate to dryness, add 5 ml of methanol to the residue to dissolve, and use it as the test solution of Shuyanqing spray.

[0051] Take 0.5 g of Shegan reference medicinal material, add 10 ml of methanol to the Shegan reference...

Embodiment 3

[0053] Example three: Quality inspection of Shuyanqing spray

[0054] (1) Take 20ml of Shuyanqing spray, shake and extract 2 times with ethyl acetate, 20ml of ethyl acetate each time, wherein the ethyl acetate layer is discarded during shaking and extraction, and the water layer is retained; the water layer is saturated with water The n-butanol solution was shaken and extracted twice, each time the water-saturated n-butanol solution was 20ml, wherein, the water layer was discarded during the shaking extraction, the n-butanol layer was retained, and the combined n-butanol layer; n-butanol layer; Shake and extract twice with a saturated aqueous solution of n-butanol, each time 20 ml of a saturated aqueous solution of n-butanol, divide the n-butanol solution, evaporate to dryness, add 5 ml of methanol to the residue to dissolve, and use it as the test solution of Shuyanqing spray.

[0055] Take 0.5 g of Shegan reference medicinal material, add 10 ml of methanol to the Shegan refe...

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Abstract

The invention discloses a quality detection method for Shuyanqing spray, wherein the detection process includes the following steps: (1) preparing a test solution of Shuyanqing spray and a reference medicinal material solution of Shegan; (2) sucking Shuyanqing The spray test solution and the dried reference medicinal material solution are respectively placed on the same silica gel G thin-layer plate, and the mixed solution of ethyl acetate, methanol and glacial acetic acid or the mixed solution of ethyl acetate, methanol and water is used as the developing agent, Unfold, take out, dry, inspect, and judge whether the quality of Shuyanqing spray is qualified according to the inspection results. The quality detection method for Shuyanqing spray of the present invention is a set of detection methods that are exclusive to Shuyanqing products, and have specificity for specific active substance components therein, which realizes the detection of the quality of Shuyanqing spray and ensures that The quality of the final product is stable, and the accuracy of the test results is also improved.

Description

technical field [0001] The invention belongs to the field of quality detection of traditional Chinese medicine preparations, in particular to a quality detection method of Shuyanqing spray. Background technique [0002] The ingredients of Shuyanqing spray are: watermelon cream, skullcap, shegan, mountain bean root, honeysuckle, parsnip, menthol, borneol, borax, Radix Scrophulariflora, Ophiopogon japonicus, licorice; properties: brown liquid; aroma, sweet taste , slightly bitter and acrid. The properties of Shuyanqing spray are: brown liquid; fragrant, sweet, slightly bitter and cool; functions and indications are: clearing heat and dispelling wind, reducing swelling and sore throat. For acute throat paralysis (acute pharyngitis or acute attack of chronic pharyngitis), symptoms include: sore throat, dry and burning throat, red and swollen uvula of pharyngeal mucosa, or difficulty swallowing. In the production process of Shuyanqing spray, strict quality testing is required f...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90G01N30/88G01N30/06G01N30/34
CPCG01N30/90G01N30/88G01N30/06G01N30/34G01N2030/884G01N2030/047
Inventor 邹节明高江林
Owner GUILIN SANJIN PHARMACEUTICALS CO LTD
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