A high-speed and high-stability reverse laser coating film and its preparation process
A preparation process, high stability technology, applied in the direction of coating, can solve the problems of poor production efficiency and stability, need more solvents, poor surface leveling, etc., to reduce costs, increase solid content, and promote the effect of leveling
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Embodiment 1
[0044] Take 1 part of acrylonitrile, 1 part of methacrylic acid, 3 parts of acrylamide, 2 parts of maleic acid, and 2 parts of isobornyl methacrylate and mix to obtain the first mixed monomer; take the epoxy resin and heat it up to 50 ℃, add alkoxysilane and catalyst, and ultrasonically react for 4 hours to obtain product A; in a dry nitrogen atmosphere, take product A and add γ-aminopropyltriethoxysilane to mix evenly, and react for 4 hours to obtain product B Take styrene and add cyclohexane to make solution C, take isoprene and add cyclohexane to make solution D, add styrene to cyclohexane, heat to 40°C for 25 minutes, add an initiator to react for 45 minutes, Add solution D, react for 45min, add solution C, react for 45min, take the reaction product and add the initiator, stir evenly, add product B, continue the reaction at 40°C for 3h, take the reactant and dry it to constant weight, and obtain the product E; take the product E Add ethylene glycol butyl ester and organic ...
Embodiment 2
[0049] Get 1.5 parts of acrylonitrile, 2 parts of methacrylic acid, 3.5 parts of acrylamide, 3.5 parts of maleic acid, and 3 parts of isobornyl methacrylate and mix to obtain the first mixed monomer; take epoxy resin and heat up to 60 ℃, add alkoxysilane and catalyst, ultrasonically react for 4.5 hours, and obtain product A; in a dry nitrogen atmosphere, take product A and add γ-aminopropyltriethoxysilane to mix evenly, react for 4.5 hours, and obtain Product B: take styrene and add cyclohexane to make solution C, take isoprene and add cyclohexane to make solution D, take another styrene and add cyclohexane, heat to 50°C for 30min, add initiator to react 60min, add solution D, react for 60min, add solution C, react for 60min, take the reaction product and add the initiator, stir evenly, add product B, continue the reaction at 50°C for 4h, take the reactant and dry to constant weight to obtain product E; Take the product E, add ethylene glycol butyl ester and organic molybdenum...
Embodiment 3
[0054] Take 2 parts of acrylonitrile, 3 parts of methacrylic acid, 4 parts of acrylamide, 5 parts of maleic acid, and 4 parts of isobornyl methacrylate and mix to obtain the first mixed monomer; take epoxy resin and heat up to 70 ℃, add alkoxysilane and catalyst, ultrasonically react for 5 hours to obtain product A; in a dry nitrogen atmosphere, take product A and add γ-aminopropyltriethoxysilane to mix evenly, react for 5 hours to obtain product B Take styrene and add cyclohexane to make solution C, take isoprene and add cyclohexane to make solution D, add styrene to cyclohexane, heat to 60°C for 35 minutes, add an initiator to react for 75 minutes, Add solution D, react for 75min, add solution C, react for 75min, take the reaction product and add the initiator, stir evenly, add product B, continue the reaction at 60°C for 5h, take the reactant and dry it to constant weight, and obtain the product E; take the product E Add ethylene glycol butyl ester and organic molybdenum, r...
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