Functional mask containing medical components and preparation method thereof
A functional mask technology, which is applied in the field of functional mask containing medical ingredients and its preparation, can solve the problems of poor solubility of chitosan and limit the application range of chitosan, so as to promote absorption, relieve skin tightness, sensory Experience great results
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[0025] The preparation step of described quaternary ammonium salt modified chitosan comprises:
[0026] Weigh chitosan and dissolve in acetic acid, stir at 25-35°C for 1.5-2.5 hours; continue to cool down to 0-5°C, then add cyanuric chloride and tetrahydrofuran, stir and react for 6-10 hours; Raise the temperature to 25-35°C, add quaternary ammonium salt, and stir for 8-12 hours; separate the solid from the liquid, wash the solid product with deionized water for 5 times, and then vacuum dry the solid product at 60-90°C for 12-24 hours Hours, quaternary ammonium salt modified chitosan was obtained.
[0027] The mass ratio of cyanuric chloride to chitosan is (0.5-2):1, and the mass ratio of quaternary ammonium salt to chitosan is (1-2):1.
[0028] Further preferably, the quaternary ammonium salt is 2,3-epoxypropyltrimethylammonium chloride and (2,3-epoxypropyl) ethyl bis (2-hydroxyethyl) ammonium chloride, 2, The weight ratio of 3-epoxypropyltrimethylammonium chloride to (2,3-...
Embodiment 1
[0051] This embodiment provides a functional facial mask containing medical ingredients. In parts by weight, its raw materials include 2 parts of chitosan, 10 parts of gelatin, 3 parts of collagen, 6 parts of glycerin, 0.3 parts of allantoin, lemon 1 part acid, 56 parts deionized water.
[0052] The chitosan is quaternary ammonium salt modified chitosan. The preparation step of quaternary ammonium salt modified chitosan comprises:
[0053] Weigh chitosan and dissolve it in acetic acid, stir at 30°C for 2 hours; continue to cool down to 0°C, then add cyanuric chloride and tetrahydrofuran, stir and react for 8 hours; raise the temperature of the reaction system to 30°C, add quaternary ammonium salt, stirred and reacted for 8 hours; the obtained product was separated from solid and liquid, and the solid product was washed 5 times with deionized water, and then the solid product was vacuum-dried at 85° C. for 20 hours to obtain quaternary ammonium salt modified chitosan.
[0054...
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