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Quality detection method of eleutherine plicata

A quality inspection method, the technology of shallots, applied in the direction of measuring devices, instruments, scientific instruments, etc.

Inactive Publication Date: 2021-07-30
广西壮族自治区食品药品检验所
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In summary, there is currently no quality standard that can guarantee the safety of red onion medication. Therefore, it is urgent to provide a content determination method that can quickly identify red onion medicinal materials and ensure its active ingredients.

Method used

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  • Quality detection method of eleutherine plicata
  • Quality detection method of eleutherine plicata
  • Quality detection method of eleutherine plicata

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Thin-layer chromatography identification method of red onion, as follows:

[0033] (1) Preparation of reference substance solution: Take an appropriate amount of shallot A reference substance, add ethanol to make a solution containing 0.2 mg of shallot A per 1 mL, as the reference substance solution.

[0034] (2) Preparation of the test solution: Take 1 g of the sample powder, add 30 mL of ethanol, ultrasonically treat for 30 minutes, filter, and concentrate the filtrate to 5 mL as the test solution.

[0035] (3) Identification: Take 5 μL each of the test solution and the reference solution, and place them on the same silica gel G thin-layer plate, and use petroleum ether (60-90°C)-ethyl formate with a volume ratio of 15:10:0.2 -Methanol mixed solution is used as developer, developed, taken out, dried, and inspected under 365nm ultraviolet light. In the chromatogram of the test product, spots of the same color appear on the positions corresponding to the chromatogram o...

Embodiment 2

[0039] The content determination method of red onion with one test and multiple evaluations is as follows:

[0040] (1) Chromatographic conditions and system adaptability test: Octadecylsilane bonded silica gel is used as filler; acetonitrile is used as mobile phase A, water is used as mobile phase B, and the set flow rate is 1.0mL / min, as shown in Table 1 below gradient elution according to the elution program; the detection wavelength is 254nm; the column temperature is 25°C; the number of theoretical plates should not be less than 5000 based on the calculation of the shallot peak.

[0041]

[0042] (2) Preparation of the reference substance solution: Take an appropriate amount of shallot reference substance, weigh it accurately, add ethanol to make a solution containing 0.4 mg of shallot in every 1 mL, and obtain the reference substance solution.

[0043] (3) Preparation of the test solution: Take about 0.1g of the sample powder, weigh it accurately, add 20mL of ethanol ...

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Abstract

The invention discloses a quality detection method of eleutherine plicata. The quality detection method comprises the following steps: carrying out qualitative analysis on the eleutherine plicata by adopting a thin-layer chromatography identification method and carrying out quantitative analysis on the eleutherine plicata by adopting a quantitative analysis of multi-components by single marker. When the quality detection method is used for analyzing the eleutherine plicata, the operation is simple, the analysis result can be quickly obtained, the evaluation is comprehensive, and a reliable guarantee is provided for the medication safety of the eleutherine plicata.

Description

technical field [0001] The invention relates to the technical field of quality detection of Chinese medicinal materials, in particular to a quality detection method of shallots. Background technique [0002] shallots ( Eleutherine plicata Herb. ) for Iridaceae ( Iridaceae ) Shallot ( Eleutherine ) plants, which are not recorded in the Chinese Pharmacopoeia, but are commonly used in Zhuang and Yao areas of Guangxi, and are also commonly used in some minority areas such as Dai, Yi, De'ang, and Li. Red onion is used as medicine with the whole plant or bulb, which can be harvested in spring and summer, used fresh or dried, also known as small red garlic, red onion, Paboliang (Dai language) and so on. Red onion is bitter in nature and cool in taste. It has the effects of clearing heat and detoxification, dispelling blood stasis, reducing swelling, and stopping bleeding. It is commonly used in folks to treat heart palpitations, dizziness, swelling and pain from bruises, vomit...

Claims

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Application Information

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IPC IPC(8): G01N30/90
CPCG01N30/90
Inventor 李丽莉黄莉莉吴桂凡黄清泉姚力
Owner 广西壮族自治区食品药品检验所
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