Rapid identification method for four kinds of high-temperature sterilized commercial milk
A high-temperature sterilization and identification method technology, which is applied in nuclear methods, measuring devices, and material analysis through optical means, can solve problems such as huge data and poor data mining results, and achieve rapid identification and reduce computing costs.
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Embodiment 1
[0037] Example 1: Model establishment and screening
[0038] Instruments and equipment:
[0039] Selected from MilkoScan produced by FOSS company TM 7RM milk composition detector (operate according to the product instruction manual).
[0040] Specific steps are as follows:
[0041] (1) Collect milk samples
[0042] Purchased in supermarkets 194 samples of multi-batch high-temperature sterilized pure milk of four brands with large sales volume in China, 140 samples of multi-batch high-temperature sterilized high-end milk of two brands, and 70 samples of high-temperature sterilized organic milk. 175 samples of two brands of multi-batch α2-β casein milk.
[0043] (2) Determination of mid-infrared spectrum
[0044] Pour the milk samples into cylindrical sample tubes with a diameter of 3.5cm and a height of 9cm to ensure that the liquid level is greater than 6cm, then bathe them in a water bath at 42°C for 15-20min, and then extend the solid optical fiber probe into the liquid...
Embodiment 2
[0065] Embodiment 2: the application of the present invention to construct the model
[0066] 36 high-temperature sterilized milk samples were taken to verify the model, and the predicted results were compared with the real results. Among them, the types of these 36 samples have been recorded in advance.
[0067] Specific steps: Using the methods of measuring spectrum and data preprocessing in Example 1, 36 milk samples were measured and processed, and the optimal model selected was used for identification.
[0068] The results are shown in Table 4.
[0069] Table 4 model application results
[0070]
[0071] The identification result is exactly the same as the real situation, and the identification accuracy rate of the present invention reaches 100% for 13 pure milks, 8 high-end milks, 5 organic milks and 10 A2-β casein milks.
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