Rapid identification method for pasteurized buffalo fresh milk and dairy cow fresh milk

A pasteurization and fresh milk technology, applied in character and pattern recognition, instruments, electrical and digital data processing, etc., can solve the problems of poor data mining results, incomplete data, huge data, etc., to achieve rapid identification, rapid detection, Overcome time-consuming effects

Pending Publication Date: 2021-08-27
HUAZHONG AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The data output by the mid-infrared spectrometer is a matrix of n×1060 (n is the sample size), the data is huge, and it is difficult to avoid data incompleteness, inconsistency, and is easily disturbed by noise (errors or outliers). Low-quality data will lead to Poor data mining results, so some method is needed to preprocess the output data

Method used

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  • Rapid identification method for pasteurized buffalo fresh milk and dairy cow fresh milk
  • Rapid identification method for pasteurized buffalo fresh milk and dairy cow fresh milk
  • Rapid identification method for pasteurized buffalo fresh milk and dairy cow fresh milk

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] Example 1: Establishment of pasteurized buffalo fresh milk and dairy cow fresh milk rapid identification method

[0038] Instruments and equipment: choose MilkoScan produced by FOSS company TM 7RM milk composition detector (operate according to the product instruction manual).

[0039] The specific operation steps are as follows:

[0040] (1) Collect milk samples

[0041] 98 samples of different batches of pasteurized fresh cow milk and 25 samples of different batches of pasteurized buffalo fresh milk were purchased in the market.

[0042] (2) Acquisition of mid-infrared spectrum (MIR)

[0043] Pour the milk samples into cylindrical sample tubes with a diameter of 3.5cm and a height of 9cm to ensure that the liquid level is greater than 6cm, then bathe them in a water bath at 42°C for 15-20min, and then extend the solid optical fiber probe into the liquid to absorb Sample detection, through the software to obtain the light transmittance of the sample.

[0044] (3) ...

Embodiment 2

[0064] Example 2: Application of Pasteurized Buffalo Fresh Milk and Cow Fresh Milk Rapid Identification Method

[0065] Take 10 pasteurized buffalo fresh milk and cow fresh milk samples to verify the model, and compare the predicted results with the real results. The types of these 10 samples have been documented in advance.

[0066] Specific method: Using the methods of measuring spectrum and data preprocessing in Example 1, using the optimal model of screening (no treatment + SVM) to predict 10 fresh milk samples. The output results are shown in Table 4.

[0067] Application results of the model in Table 4

[0068]

[0069] The result of the model identification of the present invention is exactly the same as the real situation, 3 buffalo fresh milk and 7 cow fresh milk, promptly reach 100% accuracy rate.

[0070] The spectral band used by the optimal model of the present invention is 925.92-1041.66cm -1 、1087.956-1269.282cm -1 、1292.43-1354.158cm -1 、1442.892-1539....

Embodiment 3

[0071] Example 3: Reapplication of pasteurized buffalo fresh milk and cow fresh milk rapid identification method

[0072] Take 30 pasteurized buffalo fresh milk samples and 120 dairy cow fresh milk samples to verify the model, and the method is the same as in Example 2. The output results are shown in Table 5.

[0073] Application results of the model in Table 5

[0074]

[0075] The identification accuracy rate of this model is 90% for pasteurized buffalo fresh milk, and 99.17% for pasteurized cow fresh milk, that is, the overall accuracy rate reaches 97.33%.

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Abstract

The invention belongs to the field of dairy product analysis, and particularly relates to a rapid identification method for pasteurized buffalo fresh milk and dairy cow fresh milk. The method comprises the steps of 1) collecting buffalo fresh milk and dairy cow fresh milk; 2) scanning the samples in a mid-infrared spectrum range to obtain mid-infrared spectrum data; 3) preprocessing the original mid-infrared spectrum to remove abnormal values; 4) dividing the preprocessed data set into a training set and a test set; 5) screening spectral bands for modeling; 6) combining different spectrum preprocessing and modeling algorithms, establishing an identification model, evaluating the model by using accuracy, specificity, sensitivity and AUC, and screening out a preprocessing method and modeling algorithm combination with an optimal effect; and 7) verifying the model, and evaluating the generalization ability of the model. Due to the adoption of a simple spectrum screening method, a smaller number of wave points are used for modeling, the operation cost is reduced, the optimal model is obtained through 10 identification models, and the rate and accuracy of identifying the pasteurized buffalo fresh milk and the dairy cow fresh milk are improved.

Description

technical field [0001] The invention belongs to the technical field of milk product analysis, and in particular relates to a rapid identification method for pasteurized buffalo fresh milk and cow fresh milk. Background technique [0002] Dal et al. (2018) prepared buffalo mozzarella cheese mixed with different concentrations of milk in the laboratory, and used liquid chromatography-tandem mass spectrometry to analyze the species-specific low-molecular-weight biomarkers in the quantitative milk, so as to realize the detection of adulteration. The identification of buffalo mozzarella cheese, the quantitative combination of β-carotene and ergocalciferol makes the sensitivity threshold of detection milk is 5%, this method needs centrifugation, water bath culture, extraction of analytes and other operations [3] . Francesca et al. (2019) used capillary electrophoresis to detect cow milk in buffalo milk with bovine α-lactalbumin as an adulteration marker. The minimum amount of adu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/3577G06F30/27G06K9/62G06F111/08G06F113/08
CPCG01N21/3577G06F30/27G06F2111/08G06F2113/08G06F18/2411G06F18/24323G06F18/214
Inventor 张淑君王海童南良康杨利国李翔易建明周扬梁爱心胡修忠万平民夏瑜罗雪路苏俊东张静静
Owner HUAZHONG AGRI UNIV
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