Diarylamine compound and organic electroluminescent device containing same
A compound and aromatic amine technology, applied in the field of organic electroluminescent devices, can solve the problems such as development has not been fully realized, and achieve the effects of excellent film phase stability, excellent hole migration ability, and high glass transition temperature
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[0142] Example 1: Synthesis of Compound 1
[0143]
[0144] Under the three bottles, 0.012 mol of raw materials X-1, 0.01 mol raw materials P-1, 150 ml of toluene were added, and then 5 × 10 -5 MOL PD 2 (DBA) 3 , 5 × 10 -5 Mol Trut-butyl phosphorus, 0.03 mol of tert-buthanol sodium, heated and refluxed for 12 hours, sampling point plate, and the residual removal of the aminone compound is completely reacted. Natural cooling, filtration, filtration, skeleton column (silica gel 100-200), eluate: chloroform: n-hexane = 30: 70 (volume ratio)), to obtain natural cooling to room temperature, filtration, filtrate To no distortion, a medium-sized silica gel column, resulting in an intermediate M-1, purity 98.63%, yield of 75.06%;
[0145] In three bottles, 0.01 mol intermediate M-1, 0.025 mol intermediate Q-1, 150 ml of toluene was added, and then added 5 × 10 -5 MOL PD 2 (DBA) 3 , 5 × 10 -5 Mol Trut-butyl phosphorus, 0.03 mol of tert-butanol sodium, reflow reaction for 12 hours, sampli...
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