Tooth whitening gel and preparation method thereof
A technology for tooth whitening and whitening gel is applied in the field of tooth whitening gel and its preparation, which can solve the problems of toothache for users, unsatisfactory actual effect, increase in cost and the like, achieve lasting anesthesia effect, relieve tooth pain and other discomforts Sensitivity, prevention of tooth sensitivity or pain
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0053] In some embodiments, the preparation method of the cyclodextrin-included anti-sensitizer granules includes:
[0054] Mix the antisensitizer with the organic solvent according to the ratio of solid to liquid 1g: (2-4) ml to obtain solution A;
[0055] Mix cyclodextrin and water according to the material-to-liquid ratio of 1g:(4-6)ml to obtain solution B;
[0056] The solution A was mixed with the solution B, stirred and dried.
[0057] The organic solvent is preferably ethanol.
[0058] Specifically, the antisensitizer and the organic solvent can be 1g:2ml, 1g:2.1ml, 1g:2.2ml, 1g:2.3ml, 1g:2.4ml, 1g:2.5ml, 1g:2.6ml according to the ratio of material to liquid , 1g: 2.7ml, 1g: 2.8ml, 1g: 2.9ml, 1g: 3ml, 1g: 3.1ml, 1g: 3.2ml, 1g: 3.3ml, 1g: 3.4ml, 1g: 3.5ml, 1g: 3.6ml, 1g: 3.7ml, 1g: 3.8ml, 1g: 3.9ml, 1g: 4ml.
[0059] Cyclodextrin and water can be 1g:4ml, 1g:4.1ml, 1g:4.2ml, 1g:4.3ml, 1g:4.4ml, 1g:4.5ml, 1g:4.6ml, 1g:4.7ml, 1g: 4.8ml, 1g: 4.9ml, 1g: 5ml, 1g: 5.1ml, 1...
Embodiment 1
[0076] Preparation of Cyclodextrin-Included Benzocaine:
[0077] Dissolve 16g of benzocaine in 50mL of ethanol to obtain solution A, dissolve 98g of β-cyclodextrin in 500mL of purified water at 50°C to obtain solution B, and add solution A dropwise to solution B under constant stirring. Stir at 50°C for 2 hours, and dry to obtain cyclodextrin-included benzocaine.
[0078] Preparation of tooth whitening gel (reaction condition is 2-8°C water bath):
[0079] 1. Weigh 0.15 grams of xylitol, 3 grams of benzocaine clathrated with β-cyclodextrin, and 18 grams of disodium hydrogen phosphate and dissolve them in 30 grams of water to obtain solution C;
[0080] 2. Weigh 0.15 g of menthol and add 9 g of glycerin, stir evenly to obtain solution D;
[0081] 3. Add solution A to solution B, stir and mix evenly, add 6 grams of carbomer and stir (600r / min, 60min) until the carbomer is completely dissolved to obtain solution E;
[0082] 4. Add 170 grams of hydrogen peroxide (with a hydroge...
Embodiment 2
[0104] Preparation of Cyclodextrin-Included Benzocaine:
[0105] Dissolve 20g of benzocaine in 50mL of ethanol to obtain solution A, dissolve 49g of methyl β-cyclodextrin in 500mL of 50°C purified water to obtain solution B, and add solution A dropwise to solution B under constant stirring , Stir at 50°C for 2h, and dry to obtain methyl β-cyclodextrin inclusion benzocaine.
[0106] Preparation of tooth whitening gel (reaction condition is 2-8°C water bath):
[0107] 1. Weigh 0.15 grams of xylitol, 6 grams of cyclodextrin-included benzocaine, and 9 grams of sodium hydroxide and dissolve them in 30 grams of water to obtain solution C;
[0108] 2. Weigh 0.15 g of menthol and add 18 g of propylene glycol, stir evenly to obtain solution D;
[0109] 3. Add solution A to solution B, stir and mix evenly, add 9 grams of poloxamer and stir (600r / min, 60min) until completely dissolved to obtain solution E;
[0110] 4. Add 70 grams of carbamide peroxide and 157.5 grams of water to solu...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com