Electrochemical detector
A detector and electrochemical technology, applied in the field of biological detectors, can solve the problem of high analyte concentration estimation
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example 1
[0072] The film is 130 microns thick and covered with a 60 nm thick layer of platinum. The area was defined by compressing the membrane to be 12.6 square millimeters. A 1.5 ml solution containing 0.2 molar potassium ferricyanide and 1% by weight glucose oxidase dehydrogenase was introduced into the volume defined by the membrane and allowed to evaporate the water.
[0073] The platinum layer was then connected to a potentiostat to serve as the working and counter / reference electrode. 3.0 ml of a clear solution containing 5 mM D-glucose and 0.9 wt% NaCl was dropped on a defined area of the membrane. After 20 seconds, a voltage of 300 mV was applied between the working electrode and the counter / reference electrode and the current was recorded at 0.1 second intervals for the next 30 seconds.
[0074] Figure 13 is the curve of current versus time according to the above measurements. The function ln(i / 26.9-1) was calculated using a steady state current of 26.9 mA and plotted...
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