Method for quantitatively analysing coke microcrystal unit from coke high-resolution-ration transmission electric-lens image
A technology of quantitative analysis and microcrystalline unit, applied in the direction of using radiation for material analysis, analyzing materials, measuring devices, etc., can solve the problem that it is difficult to make substantial progress in coke performance interpretation, and achieve the effect of deepening understanding
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[0018] The following steps are for quantitative analysis of coke microcrystalline units on the HRTEM image of Liulin coal coke samples:
[0019] 1. Streak calibration and numbering, use graphics software to calibrate and number each stripe in the figure, see Figure 1.
[0020] 2. Determine the judgment parameters of each stripe. The area A of the stripe can be determined by counting the number of pixels in each stripe. The stripes in Figure 1 are single-pixel "thick", and the calculation of the area A is determined by the number of pixels. Therefore, this area is actually the length L of the stripes, and the length L is calculated by the following formula,
[0021] L(nm)=30(1 / nm)×A(nm 2 )
[0022] 30 is the sizing factor in this embodiment.
[0023] By fitting an ellipse to the stripe, determine the center of the ellipse, approximate it to the stripe's location coordinates (x, y), and the major axis r a and minor axis r b , and the inclination angle θ of the...
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